1-amino-3-methyl-2,3-dihydro-7H-dibenzisoquinoline-2,7-dione

Base Information

Chemical Name:1-amino-3-methyl-2,3-dihydro-7H-dibenzisoquinoline-2,7-dione
CAS No.:35305-14-7
Molecular Formula:C₁₇H₁₂N₂O₂
Molecular Weight:276.294
Hs Code.:

1-amino-3-methyl-2,3-dihydro-7H-dibenz<f,ij>isoquinoline-2,7-dione

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-amino-3-methyl-2,3-dihydro-7H-dibenzisoquinoline-2,7-dione

Chemical Property:

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Technology Process of 1-amino-3-methyl-2,3-dihydro-7H-dibenzisoquinoline-2,7-dione

There total 1 articles about 1-amino-3-methyl-2,3-dihydro-7H-dibenzisoquinoline-2,7-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 62-53-3
aniline

: 3-methyl-2,7-dioxo-2,3-dihydro-7H-dibenzisoquinoline-1-diasonium hydrogen sulfate

: 35305-14-7
1-amino-3-methyl-2,3-dihydro-7H-dibenzisoquinoline-2,7-dione

: 59836-57-6
1-anilino-3-methyl-3H-naphtho[1,2,3-de]quinoline-2,7-dione

Guidance literature:: In water; acetone; at 60 ℃;

Reference yield:

: 35305-14-7
1-amino-3-methyl-2,3-dihydro-7H-dibenzisoquinoline-2,7-dione

: C₂₄H₁₈N₄O₂

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / nitrosylsulfuric acid, glac. AcOH / 2 h / Ambient temperature

2: aq. acetic acid

With nitrosylsulfuric acid; acetic acid; In acetic acid;

Reference yield:

: 35305-14-7
1-amino-3-methyl-2,3-dihydro-7H-dibenzisoquinoline-2,7-dione

: C₂₅H₂₀N₄O₂

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / nitrosylsulfuric acid, glac. AcOH / 2 h / Ambient temperature

2: 66 percent / acetone; H₂O / Ambient temperature

With nitrosylsulfuric acid; acetic acid; In water; acetone;