C₁₄H₂₀F₂N₂O₂S

Base Information

Chemical Name:C₁₄H₂₀F₂N₂O₂S
CAS No.:1292322-06-5
Molecular Formula:C₁₄H₂₀F₂N₂O₂S
Molecular Weight:318.388
Hs Code.:

C<sub>14</sub>H<sub>20</sub>F<sub>2</sub>N<sub>2</sub>O<sub>2</sub>S

Synonyms:

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Chemical Property of C₁₄H₂₀F₂N₂O₂S

Chemical Property:

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Technology Process of C₁₄H₂₀F₂N₂O₂S

There total 13 articles about C₁₄H₂₀F₂N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₈F₂N₂O₄S

: 1292322-06-5
C₁₄H₂₀F₂N₂O₂S

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: C₁₄H₂₀Cl₃NO₅

: 1292322-06-5
C₁₄H₂₀F₂N₂O₂S

Guidance literature:: Multi-step reaction with 10 steps

1: n-butyllithium / tetrahydrofuran / -78 °C

2: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

3: hydrogenchloride / methanol / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

6: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

7: chloro-trimethyl-silane / dichloromethane / 20 °C

8: palladium 10% on activated carbon; hydrogen / ethanol

9: triethylamine / dichloromethane / 20 °C

10: hydrogenchloride / methanol / 20 °C

With hydrogenchloride; n-butyllithium; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 6: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 1292321-47-1
C₂₉H₃₄F₂N₂O₅

: 1292322-06-5
C₁₄H₂₀F₂N₂O₂S

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / methanol / 20 °C

2: triethylamine / dichloromethane / 20 °C

3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

4: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

5: chloro-trimethyl-silane / dichloromethane / 20 °C

6: palladium 10% on activated carbon; hydrogen / ethanol

7: triethylamine / dichloromethane / 20 °C

8: hydrogenchloride / methanol / 20 °C

With hydrogenchloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060