Technology Process of C19H25NO7S
There total 7 articles about C19H25NO7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / 24 h / 0 - 4 °C / Inert atmosphere
2: triethylamine / dichloromethane / 15 h / 20 °C
3: methanol / 5 h / 20 °C
4: trifluoroacetic acid / water / 1 h / 0 - 20 °C
5: palladium 10% on activated carbon; hydrogen; ammonium formate / methanol / 1 h / Reflux
6: pyridine / 6 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; ammonium formate; triethylamine; trifluoroacetic acid;
In
pyridine; methanol; dichloromethane; water;
3: Michael condensation;
DOI:10.1021/jo101877r
- Guidance literature:
-
Multi-step reaction with 7 steps
1: magnesium bis(monoperoxyphthalate) hexahydrate / methanol / 6 h / 20 °C / Inert atmosphere
2: pyridine / 24 h / 0 - 4 °C / Inert atmosphere
3: triethylamine / dichloromethane / 15 h / 20 °C
4: methanol / 5 h / 20 °C
5: trifluoroacetic acid / water / 1 h / 0 - 20 °C
6: palladium 10% on activated carbon; hydrogen; ammonium formate / methanol / 1 h / Reflux
7: pyridine / 6 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; ammonium formate; magnesium bis(monoperoxyphthalate) hexahydrate; triethylamine; trifluoroacetic acid;
In
pyridine; methanol; dichloromethane; water;
4: Michael condensation;
DOI:10.1021/jo101877r
- Guidance literature:
-
Multi-step reaction with 4 steps
1: methanol / 5 h / 20 °C
2: trifluoroacetic acid / water / 1 h / 0 - 20 °C
3: palladium 10% on activated carbon; hydrogen; ammonium formate / methanol / 1 h / Reflux
4: pyridine / 6 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; ammonium formate; trifluoroacetic acid;
In
pyridine; methanol; water;
1: Michael condensation;
DOI:10.1021/jo101877r