Technology Process of C16H15NO3
There total 5 articles about C16H15NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
DOI:10.1021/ja204924j
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1H-imidazole / tetrahydrofuran / 20 °C / Inert atmosphere
2: N-Bromosuccinimide / dichloromethane
3: water; sodium hydroxide / dichloromethane; N,N-dimethyl-formamide / 20 °C
4: N-[menthyloxycarbonyl]-L-leucine; silver(I) acetate; palladium diacetate; lithium carbonate / 1,2-dichloro-ethane / 24 h / 100 °C / Inert atmosphere
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
With
1H-imidazole; N-Bromosuccinimide; N-[menthyloxycarbonyl]-L-leucine; tetrabutyl ammonium fluoride; water; silver(I) acetate; palladium diacetate; lithium carbonate; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja204924j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; sodium hydroxide / dichloromethane; N,N-dimethyl-formamide / 20 °C
2: N-[menthyloxycarbonyl]-L-leucine; silver(I) acetate; palladium diacetate; lithium carbonate / 1,2-dichloro-ethane / 24 h / 100 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
With
N-[menthyloxycarbonyl]-L-leucine; tetrabutyl ammonium fluoride; water; silver(I) acetate; palladium diacetate; lithium carbonate; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja204924j