2-((E)-2-Methyl-3-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-propenyl)-5-(4-methylsulfanyl-phenyl)-1H-imidazole

Base Information

Chemical Name:2-((E)-2-Methyl-3-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-propenyl)-5-(4-methylsulfanyl-phenyl)-1H-imidazole
CAS No.:1053474-17-1
Molecular Formula:C₃₅H₆₀N₂O₅SSi₃
Molecular Weight:705.194
Hs Code.:

2-((E)-2-Methyl-3-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-propenyl)-5-(4-methylsulfanyl-phenyl)-1H-imidazole

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Chemical Property of 2-((E)-2-Methyl-3-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-propenyl)-5-(4-methylsulfanyl-phenyl)-1H-imidazole

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Technology Process of 2-((E)-2-Methyl-3-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-propenyl)-5-(4-methylsulfanyl-phenyl)-1H-imidazole

There total 5 articles about 2-((E)-2-Methyl-3-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-propenyl)-5-(4-methylsulfanyl-phenyl)-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93554-85-9
Amino-(4-methylsulfanyl-phenyl)-acetonitrile

: 1053474-17-1
2-((E)-2-Methyl-3-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-propenyl)-5-(4-methylsulfanyl-phenyl)-1H-imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / tetrahydrofuran / Ambient temperature

2: Et₃N, 4-(N,N-dimethylamino)pyridine / tetrahydrofuran / 1 h / 20 °C

3: 1.) diisobutylaluminium hydride, 2.) Et₃N, triphenylphosphine dibromide / 1) THF, -78 deg C, 1 h; 2) THF, 0 deg C, 70 min;

With dmap; diisobutylaluminium hydride; triethylamine; dibromotriphenylphosphorane; In tetrahydrofuran;

Reference yield:

: 66262-68-8,66290-01-5,70470-39-2
monic acid A

: 1053474-17-1
2-((E)-2-Methyl-3-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-propenyl)-5-(4-methylsulfanyl-phenyl)-1H-imidazole

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / tetrahydrofuran / 0.5 h / -10 °C

2: 54 percent / tetrahydrofuran / Ambient temperature

3: Et₃N, 4-(N,N-dimethylamino)pyridine / tetrahydrofuran / 1 h / 20 °C

4: 1.) diisobutylaluminium hydride, 2.) Et₃N, triphenylphosphine dibromide / 1) THF, -78 deg C, 1 h; 2) THF, 0 deg C, 70 min;

With dmap; diisobutylaluminium hydride; triethylamine; dibromotriphenylphosphorane; In tetrahydrofuran;

Reference yield:

: 79959-72-1
monic acid isobutyryl carbonic anhydride

: 1053474-17-1
2-((E)-2-Methyl-3-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-propenyl)-5-(4-methylsulfanyl-phenyl)-1H-imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / tetrahydrofuran / Ambient temperature

2: Et₃N, 4-(N,N-dimethylamino)pyridine / tetrahydrofuran / 1 h / 20 °C

3: 1.) diisobutylaluminium hydride, 2.) Et₃N, triphenylphosphine dibromide / 1) THF, -78 deg C, 1 h; 2) THF, 0 deg C, 70 min;

With dmap; diisobutylaluminium hydride; triethylamine; dibromotriphenylphosphorane; In tetrahydrofuran;