Technology Process of Cyclohexanol,2,6-diamino-,(1alpha,2alpha,6beta)-(9CI)
There total 6 articles about Cyclohexanol,2,6-diamino-,(1alpha,2alpha,6beta)-(9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 20 ℃;
for 9h;
under 3102.97 Torr;
DOI:10.1021/jo100724w
- Guidance literature:
-
With
ammonium hydroxide;
In
ethanol;
at 100 ℃;
for 1h;
sealed steel tube;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99 percent / sodium borohydride / propan-2-ol; H2O / 1 h / 0 deg C -> room temperature
2: 87 percent / NBS / CHCl3 / 1 h / Ambient temperature
3: 92 percent / silver oxide / tetrahydrofuran / 8 h / Ambient temperature; dark
4: 35percent aq. ammonia / ethanol / 1 h / 100 °C / sealed steel tube
With
ammonium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; silver(l) oxide;
In
tetrahydrofuran; ethanol; chloroform; water; isopropyl alcohol;
