5-methyl-7-(2,2,6-trimethyl-cyclohexyl)-heptanoic acid

Base Information

• Chemical Name: 5-methyl-7-(2,2,6-trimethyl-cyclohexyl)-heptanoic acid
• CAS No.: 93479-49-3
• Molecular Formula: C₁₇H₃₂O₂
• Molecular Weight: 268.44
• Mol file: 93479-49-3.mol

Synonyms:

Chemical Property of 5-methyl-7-(2,2,6-trimethyl-cyclohexyl)-heptanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-methyl-7-(2,2,6-trimethyl-cyclohexyl)-heptanoic acid

There total 7 articles about 5-methyl-7-(2,2,6-trimethyl-cyclohexyl)-heptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nitril d. 4-Methyl-6-(2,6,6-trimethyl-cyclohexen-1-yl)-hexen-3-in-5-carbonsaeure-(1) (93477-20-4) → 5-methyl-7-(2,2,6-trimethyl-cyclohexyl)-heptanoic acid (93479-49-3)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / methanol

2: H₂ / Pt

With potassium hydroxide; hydrogen; platinum; In methanol;

Reference yield:

sodium diethylmalonate (996-82-7,34727-00-9,73177-21-6) + 2-(5-bromo-3-methyl-pentyl)-1,1,3-trimethyl-cyclohexane (859819-62-8) → 5-methyl-7-(2,2,6-trimethyl-cyclohexyl)-heptanoic acid (93479-49-3)

Guidance literature:

With ethanol; at 150 ℃; Erwaermen des Reaktionsgemisches mit methanol. Kalilauge und Erhitzen der gebildeten Dicarbonsaeure unter vermindertem Druck bis auf 230grad;

DOI:10.1002/hlca.19330160192 DOI:10.1002/hlca.19330160176

Reference yield:

4-Methyl-6-(2,6,6-trimethyl-cyclohexen-1-yl)-hexen-3-in-5-carbonsaeure-(1) (96579-58-7) → 5-methyl-7-(2,2,6-trimethyl-cyclohexyl)-heptanoic acid (93479-49-3)

Guidance literature:

With hydrogen; platinum;

upstream raw materials:

sodium diethylmalonate

2-(5-bromo-3-methyl-pentyl)-1,1,3-trimethyl-cyclohexane

(2E,4E,6E)-5-Methyl-7-(2,6,6-trimethyl-cyclohex-1-enyl)-hepta-2,4,6-trienoic acid

5-methyl-7t-(2,6,6-trimethyl-cyclohex-1-enyl)-hepta-2t,4c,6-trienoic acid