13C-labeled tetraphenylphosphonium bromide

Base Information

• Chemical Name: 13C-labeled tetraphenylphosphonium bromide
• CAS No.: 1466545-66-3
• Molecular Formula: Br*C₂₄H₂₀P
• Molecular Weight: 425.235

Synonyms:

Chemical Property of 13C-labeled tetraphenylphosphonium bromide

Chemical Property:

Purity/Quality:

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Technology Process of 13C-labeled tetraphenylphosphonium bromide

There total 1 articles about 13C-labeled tetraphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenylphosphine (603-35-0) + bromobenzene-1,2,3,4,5,6-13C6 (112630-77-0,287399-23-9) → 13C-labeled tetraphenylphosphonium bromide (1466545-66-3)

Guidance literature:

With nickel dibromide; In ethylene glycol; at 180 ℃; for 4h; Sealed tube;

DOI:10.1021/ja402605s

upstream raw materials:

triphenylphosphine

bromobenzene-1,2,3,4,5,6-¹³C₆

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