Methyl-phosphonic acid (R)-1-((S)-1-dibenzylamino-ethyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2,2-dimethyl-propyl ester 2-trimethylsilanyl-ethyl ester

Base Information

Chemical Name:Methyl-phosphonic acid (R)-1-((S)-1-dibenzylamino-ethyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2,2-dimethyl-propyl ester 2-trimethylsilanyl-ethyl ester
CAS No.:208765-07-5
Molecular Formula:C₃₅H₄₇N₂O₅PSi
Molecular Weight:634.828
Hs Code.:

Methyl-phosphonic acid (R)-1-((S)-1-dibenzylamino-ethyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2,2-dimethyl-propyl ester 2-trimethylsilanyl-ethyl ester

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Chemical Property of Methyl-phosphonic acid (R)-1-((S)-1-dibenzylamino-ethyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2,2-dimethyl-propyl ester 2-trimethylsilanyl-ethyl ester

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Technology Process of Methyl-phosphonic acid (R)-1-((S)-1-dibenzylamino-ethyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2,2-dimethyl-propyl ester 2-trimethylsilanyl-ethyl ester

There total 4 articles about Methyl-phosphonic acid (R)-1-((S)-1-dibenzylamino-ethyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2,2-dimethyl-propyl ester 2-trimethylsilanyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85-44-9
phthalic anhydride

: 208765-07-5
Methyl-phosphonic acid (R)-1-((S)-1-dibenzylamino-ethyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2,2-dimethyl-propyl ester 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / toluene / Heating

2: 1) 1H-tetrazole, DIPEA / 1) benzene, room temperature, overnight, 2) benzene, 15 min

With 1H-tetrazole; N-ethyl-N,N-diisopropylamine; In toluene;
DOI:10.1080/00397919808006864

Reference yield:

: 195207-46-6
4-(S)-(N,N-dibenzylamino)-2,2-dimethyl-3-(R)-hydroxynpentanenitrile

: 208765-07-5
Methyl-phosphonic acid (R)-1-((S)-1-dibenzylamino-ethyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2,2-dimethyl-propyl ester 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / LiAlH₄ / diethyl ether / 1 h / 0 °C

2: 66 percent / toluene / Heating

3: 1) 1H-tetrazole, DIPEA / 1) benzene, room temperature, overnight, 2) benzene, 15 min

With 1H-tetrazole; lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; In diethyl ether; toluene;
DOI:10.1080/00397919808006864

Reference yield:

: 208765-03-1
(3R,4S)-1-Amino-4-dibenzylamino-2,2-dimethyl-pentan-3-ol

: 208765-07-5
Methyl-phosphonic acid (R)-1-((S)-1-dibenzylamino-ethyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2,2-dimethyl-propyl ester 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / toluene / Heating

2: 1) 1H-tetrazole, DIPEA / 1) benzene, room temperature, overnight, 2) benzene, 15 min

With 1H-tetrazole; N-ethyl-N,N-diisopropylamine; In toluene;
DOI:10.1080/00397919808006864