Zn₃(S(CH₂C₇H₄N₂CH₃)2)(SCH₂C₆H₅)6

Base Information

• Chemical Name: Zn₃(S(CH₂C₇H₄N₂CH₃)2)(SCH₂C₆H₅)6
• CAS No.: 206977-23-3
• Molecular Formula: C₆₀H₆₀N₄S₇Zn₃
• Molecular Weight: 1257.8

Synonyms:

Chemical Property of Zn₃(S(CH₂C₇H₄N₂CH₃)2)(SCH₂C₆H₅)6

Chemical Property:

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Technology Process of Zn₃(S(CH₂C₇H₄N₂CH₃)2)(SCH₂C₆H₅)6

There total 1 articles about Zn₃(S(CH₂C₇H₄N₂CH₃)2)(SCH₂C₆H₅)6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

zinc nitrate tetrahydrate + phenylmethanethiol (100-53-8) + 1,3-bis(1-methylbenzimidazol-2-yl)-2-thiapropane → Zn3(S(CH2C7H4N2CH3)2)(SCH2C6H5)6 (206977-23-3)

Guidance literature:

With NaOMe; In methanol; inert atmosphere, stoich. amts.; treatment of PhCH2SH with NaOMe, slow addn. of Zn-salt (over 1 h, stirring), addn. of benzimidazole derivative,stirring for 1 h; vol. reduction (vac.), standing for 1 week (pptn.), collection (filtration), washing (ice cold MeOH), drying (vac.), recrystn. (hot MeCN), drying (vac., several h);

DOI:10.1021/ic971402j

upstream raw materials:

phenylmethanethiol

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