cis-dichloro(6-aminomethylnicotinic acid aniline amide)platinum(II)

Base Information

Chemical Name:cis-dichloro(6-aminomethylnicotinic acid aniline amide)platinum(II)
CAS No.:863014-16-8
Molecular Formula:C₁₃H₁₃Cl₂N₃OPt
Molecular Weight:493.252
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Chemical Property of cis-dichloro(6-aminomethylnicotinic acid aniline amide)platinum(II)

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Technology Process of cis-dichloro(6-aminomethylnicotinic acid aniline amide)platinum(II)

There total 1 articles about cis-dichloro(6-aminomethylnicotinic acid aniline amide)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 863014-11-3
cis-dichloro(6-aminomethylnicotinic acid)platinum(II)

: 62-53-3
aniline

: 863014-16-8
cis-dichloro(6-aminomethylnicotinic acid aniline amide)platinum(II)

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; In N,N-dimethyl-formamide; under exclusion of air and moisture; soln. of Pt complex (0.24 mmol) in dry DMF (15 ml) cooled to 0°C; treated with NEt3 (0.24 mmol) and ClCO2Et (0.26 mmol); stirred (30 min, 0°C); aniline (0.24 mmol) added; stirred (12 h, room temp.); MeOH-CH2Cl2 (1:20 v/v, 50 ml) added; extd. with H2O (20 ml); aq. phase re-extd. with above mixt. (5x20 ml); org. phase concd. (vac.); residue purified by column chromy. (silica gel 60, CH2Cl2-acetone 1:1 v/v); elem. anal.;
DOI:10.1016/j.ica.2005.05.015