5,7,7-trimethyl-6,8-dioxabicyclo[3.2.1]octane

Base Information

• Chemical Name: 5,7,7-trimethyl-6,8-dioxabicyclo[3.2.1]octane
• CAS No.: 16566-96-4
• Molecular Formula: C9H16 O2
• Molecular Weight: 156.225

Synonyms:NSC 328730

Chemical Property of 5,7,7-trimethyl-6,8-dioxabicyclo[3.2.1]octane

Chemical Property:

• Vapor Pressure: 1.07mmHg at 25°C
• Boiling Point: 183.1°C at 760 mmHg
• Flash Point: 62°C
• Density: 0.987g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,7,7-trimethyl-6,8-dioxabicyclo[3.2.1]octane

There total 1 articles about 5,7,7-trimethyl-6,8-dioxabicyclo[3.2.1]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-acetyl-6-methyl-2,3-dihydropyran (28450-02-4) + trimethylaluminum (75-24-1) → 5,7,7-trimethyl-6,8-dioxabicyclo<3.2.1>octane (16566-96-4)

Guidance literature:

With toluene-4-sulfonic acid; Yield given. Multistep reaction; 1) CH₂Cl₂, 0 deg C, 20 h; 2) benzene;

Reference yield: 80.0%

5,7,7-trimethyl-6,8-dioxabicyclo<3.2.1>octane (16566-96-4) → 3-isopropyl-2-cyclohexen-1-one (6328-22-9)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; In dichloromethane; for 15h; Heating;

DOI:10.1002/jhet.5570340151

Reference yield: 80.0%

5,7,7-trimethyl-6,8-dioxabicyclo<3.2.1>octane (16566-96-4) → 2,2,3-trimethyl-3-cyclohexen-1-one

Guidance literature:

With chloro-trimethyl-silane; sodium iodide; In acetonitrile; for 20h; Heating;

DOI:10.1081/SCC-100103320

upstream raw materials:

2-acetyl-6-methyl-2,3-dihydropyran

trimethylaluminum

Downstream raw materials:

3-isopropyl-2-cyclohexen-1-one

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 16566-96-4 5,7,7-trimethyl-6,8-dioxabicyclo[3.2.1]octane

Send

Send

Metric Ton KG G Pound L ML

Send

Send