2,3-dihydroxycyclopentyl benzyl ether

Base Information

Chemical Name:2,3-dihydroxycyclopentyl benzyl ether
CAS No.:62894-12-6
Molecular Formula:C₁₂H₁₆O₃
Molecular Weight:208.257
Hs Code.:

Synonyms:

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Chemical Property of 2,3-dihydroxycyclopentyl benzyl ether

Chemical Property:

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Technology Process of 2,3-dihydroxycyclopentyl benzyl ether

There total 4 articles about 2,3-dihydroxycyclopentyl benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.7%

: 68241-89-4
[(cyclopent-2-en-1-yloxy)methyl]benzene

: 62894-12-6,62960-21-8,62960-24-1,62960-25-2
2,3-dihydroxycyclopentyl benzyl ether

Guidance literature:: With potassium citrate; potassium carbonate; 4-methylmorpholine N-oxide; In water; acetonitrile; at 20 ℃; for 12.5h; Cooling with ice;

Reference yield:

: 3212-60-0,6426-28-4,62894-08-0,109431-72-3
cyclopent-2-enol

: 62894-12-6,62960-21-8,62960-24-1,62960-25-2
2,3-dihydroxycyclopentyl benzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutylammomium bromide / tetrahydrofuran / 0.08 h / -5 °C

1.2: 0.17 h / -5 °C

1.3: 5.5 h / 20 °C

2.1: 4-methylmorpholine N-oxide; potassium citrate; potassium carbonate / acetonitrile; water / 12.5 h / 20 °C / Cooling with ice

With tetrabutylammomium bromide; potassium citrate; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; acetonitrile;

Reference yield:

: 930-30-3
cyclopent-2-enone

: 62894-12-6,62960-21-8,62960-24-1,62960-25-2
2,3-dihydroxycyclopentyl benzyl ether

Guidance literature:: Multi-step reaction with 3 steps

1.1: ruthenium trichloride / methanol / 0.5 - 10 °C

1.2: 2 h / -10 °C

2.1: tetrabutylammomium bromide / tetrahydrofuran / 0.08 h / -5 °C

2.2: 0.17 h / -5 °C

2.3: 5.5 h / 20 °C

3.1: 4-methylmorpholine N-oxide; potassium citrate; potassium carbonate / acetonitrile; water / 12.5 h / 20 °C / Cooling with ice

With ruthenium trichloride; tetrabutylammomium bromide; potassium citrate; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; water; acetonitrile;