1,1'-ferrocenediyldibenzyloxysilane

Base Information

• Chemical Name: 1,1'-ferrocenediyldibenzyloxysilane
• CAS No.: 208509-79-9
• Molecular Formula: C₂₄H₂₂FeO₂Si
• Molecular Weight: 426.37

Synonyms:

Chemical Property of 1,1'-ferrocenediyldibenzyloxysilane

Chemical Property:

Purity/Quality:

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Technology Process of 1,1'-ferrocenediyldibenzyloxysilane

There total 1 articles about 1,1'-ferrocenediyldibenzyloxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1,1-dichloro-1-sila-[1]ferrocenophane + benzyl alcohol (100-51-6,185532-71-2) → 1,1'-ferrocenediyldibenzyloxysilane (208509-79-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; byproducts: triethylammonium chloride; under Ar, vac. line and Schlenk techniques; 2 equiv. of Et3N added to soln. of Fe complex in THF; cooled to 0°C in ice bath; soln. of 2 equiv. of PhCH2OH in THF added dropwise over 2 h; stirred for 7 h at ambient temp.; solvent evapd. in vac.; dissolved in pentane; filtered; filtrate concd. under vac.; gently warmed to homogeneity; crystd. at -18°C; recrystd.; elem. anal.;

DOI:10.1016/S0022-328X(00)00749-X

Reference yield:

1,1'-ferrocenediyldibenzyloxysilane (208509-79-9) → (C5H4)Fe(C5H4Si(OCH2C6H5)2)

Guidance literature:

In solid; under Ar, vac. line and Schlenk techniques; in vac. sealed Pyrex tube; ring-opening polymerisation at 180°C for ca. 1 h; Soxlet extd. with pentane; elem. anal.;

DOI:10.1016/S0022-328X(00)00749-X

upstream raw materials:

benzyl alcohol

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