trans-1,3-dimethyl-indane

Base Information

• Chemical Name: trans-1,3-dimethyl-indane
• CAS No.: 116384-75-9
• Molecular Formula: C₁₁H₁₄
• Molecular Weight: 146.232
• Mol file: 116384-75-9.mol

Synonyms:

Chemical Property of trans-1,3-dimethyl-indane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-1,3-dimethyl-indane

There total 24 articles about trans-1,3-dimethyl-indane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C12H16O3S → cis-1,3-dimethylindane (26561-33-1) + trans-1,3-dimethyl-indane (4175-53-5,26561-33-1,40324-83-2,116384-74-8,116384-75-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 2h; optical yield given as %de; Reflux;

DOI:10.1021/ol8023105

Reference yield:

2-(2-iodo-1-methylethyl)styrene (409334-02-7) → cis-1,3-dimethylindane (26561-33-1) + trans-1,3-dimethyl-indane (4175-53-5,26561-33-1,40324-83-2,116384-74-8,116384-75-9)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 10h; Heating;

Reference yield:

1,3-dimethyl-1-indanol (241155-65-7) → cis-1,3-dimethylindane (26561-33-1) + trans-1,3-dimethyl-indane (4175-53-5,26561-33-1,40324-83-2,116384-74-8,116384-75-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In chloroform; for 16h; under 760 Torr; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1071/CH9900329

upstream raw materials:

1,3-dimethyl-1-indanol

trans-1,3-dimethylindan-1-ol

(+)-1,3-Dimethyl-inden

4-(o-bromophenyl)pent-1-ene

Downstream raw materials:

(+/-)-trans-trikentrin A