Tetraacetylclionamid

Base Information

Chemical Name:Tetraacetylclionamid
CAS No.:68857-44-3
Molecular Formula:C₂₇H₂₆BrN₃O₈
Molecular Weight:600.423
Hs Code.:

Synonyms:

Suppliers and Price of Tetraacetylclionamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tetraacetylclionamid

Chemical Property:

Purity/Quality:

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Technology Process of Tetraacetylclionamid

There total 21 articles about Tetraacetylclionamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70475-59-1
3,4,5-triacetoxybenzoyl chloride

: 68857-44-3
Tetraacetylclionamid

Guidance literature:: Multi-step reaction with 9 steps

1: 97 percent / NEt₃ / dioxane; diethyl ether / 12 h / 0 °C

2: 92 percent / 1N HCl / dioxane; diethyl ether / 0.25 h / 10 °C

3: 83 percent / KI, NaN₃ / acetone / 2 h / Ambient temperature

4: 0.5N HCl, H₂ / Pd/C (5percent) / ethanol; diethyl ether / 1 h / 2250.2 Torr

5: 86 percent / NEt₃ / 0.5 h / 0 °C

6: 90 percent / NaCNBH₃ / ethyl acetate; tetrahydrofuran / 12 h / Ambient temperature

7: 86 percent / tri-n-butylphosphan / tetrahydrofuran / 0 °C

8: 79 percent / sodium-metaperiodate / tetrahydrofuran; methanol; H₂O / 3 h / Ambient temperature

9: 1) THF, 2) KHCO₃ / 1) 1,3-dimethoxybenzene, 0 deg C, 15 min, 2) ethylacetate, 3h, r.t.

With tetrahydrofuran; hydrogenchloride; sodium periodate; sodium azide; tributylphosphine; hydrogen; sodium cyanoborohydride; potassium hydrogencarbonate; triethylamine; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; water; ethyl acetate; acetone;
DOI:10.1002/jlac.198519850414

Reference yield:

: 97443-98-6
2-Chlor-1-(3,4,5-triacetoxyphenyl)ethanon

: 68857-44-3
Tetraacetylclionamid

Guidance literature:: Multi-step reaction with 7 steps

1: 83 percent / KI, NaN₃ / acetone / 2 h / Ambient temperature

2: 0.5N HCl, H₂ / Pd/C (5percent) / ethanol; diethyl ether / 1 h / 2250.2 Torr

3: 86 percent / NEt₃ / 0.5 h / 0 °C

4: 90 percent / NaCNBH₃ / ethyl acetate; tetrahydrofuran / 12 h / Ambient temperature

5: 86 percent / tri-n-butylphosphan / tetrahydrofuran / 0 °C

6: 79 percent / sodium-metaperiodate / tetrahydrofuran; methanol; H₂O / 3 h / Ambient temperature

7: 1) THF, 2) KHCO₃ / 1) 1,3-dimethoxybenzene, 0 deg C, 15 min, 2) ethylacetate, 3h, r.t.

With tetrahydrofuran; hydrogenchloride; sodium periodate; sodium azide; tributylphosphine; hydrogen; sodium cyanoborohydride; potassium hydrogencarbonate; triethylamine; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; ethyl acetate; acetone;
DOI:10.1002/jlac.198519850414

Reference yield:

: 97443-97-5
2-Diazo-1-(3,4,5-triacetoxyphenyl)ethanon

: 68857-44-3
Tetraacetylclionamid

Guidance literature:: Multi-step reaction with 8 steps

1: 92 percent / 1N HCl / dioxane; diethyl ether / 0.25 h / 10 °C

2: 83 percent / KI, NaN₃ / acetone / 2 h / Ambient temperature

3: 0.5N HCl, H₂ / Pd/C (5percent) / ethanol; diethyl ether / 1 h / 2250.2 Torr

4: 86 percent / NEt₃ / 0.5 h / 0 °C

5: 90 percent / NaCNBH₃ / ethyl acetate; tetrahydrofuran / 12 h / Ambient temperature

6: 86 percent / tri-n-butylphosphan / tetrahydrofuran / 0 °C

7: 79 percent / sodium-metaperiodate / tetrahydrofuran; methanol; H₂O / 3 h / Ambient temperature

8: 1) THF, 2) KHCO₃ / 1) 1,3-dimethoxybenzene, 0 deg C, 15 min, 2) ethylacetate, 3h, r.t.

With tetrahydrofuran; hydrogenchloride; sodium periodate; sodium azide; tributylphosphine; hydrogen; sodium cyanoborohydride; potassium hydrogencarbonate; triethylamine; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; water; ethyl acetate; acetone;
DOI:10.1002/jlac.198519850414