N--O-<2,2,2-trifluor-1-benzyloxycarbonylamino-aethyl>-Ser

Base Information

Chemical Name:N--O-<2,2,2-trifluor-1-benzyloxycarbonylamino-aethyl>-Ser
CAS No.:17896-40-1
Molecular Formula:C₁₈H₂₃F₃N₂O₇
Molecular Weight:436.385
Hs Code.:

N-<tert.-Butyloxycarbonyl>-O-<2,2,2-trifluor-1-benzyloxycarbonylamino-aethyl>-Ser

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Chemical Property of N--O-<2,2,2-trifluor-1-benzyloxycarbonylamino-aethyl>-Ser

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Technology Process of N--O-<2,2,2-trifluor-1-benzyloxycarbonylamino-aethyl>-Ser

There total 1 articles about N--O-<2,2,2-trifluor-1-benzyloxycarbonylamino-aethyl>-Ser which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3262-72-4
(S)-N-(tert-butoxycarbonyl)serine

: 2,2,2-Trifluor-1-chlor-N-benzyloxycarbonyl-ethylamin

: 17896-40-1
N--O-<2,2,2-trifluor-1-benzyloxycarbonylamino-aethyl>-Ser

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1002/cber.19681010323

Reference yield:

: 17896-40-1
N--O-<2,2,2-trifluor-1-benzyloxycarbonylamino-aethyl>-Ser

: 17993-39-4
N--O-<2.2.2-trifluor-1-benzyloxycarbonylaminoaethyl>-Ser-O-<2.2.2-trifluor-1-benzyloxycarbonylaminoaethyl>-Ser-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: DCC, Et₃N / CH₂Cl₂

2: Et₃N / tetrahydrofuran

With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/cber.19681010323

Reference yield:

: 17896-40-1
N--O-<2,2,2-trifluor-1-benzyloxycarbonylamino-aethyl>-Ser

: (1-{(S)-2-[(S)-2-(1-Benzyloxycarbonylamino-2,2,2-trifluoro-ethoxy)-1-hydrazinocarbonyl-ethylcarbamoyl]-2-tert-butoxycarbonylamino-ethoxy}-2,2,2-trifluoro-ethyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: DCC, Et₃N / CH₂Cl₂

2: Et₃N / tetrahydrofuran

3: N₂H₄*H₂O / methanol / Heating

With hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/cber.19681010323