HOC₆H₂Br₂CHNC₆H₄B(OH)2

Base Information

• Chemical Name: HOC₆H₂Br₂CHNC₆H₄B(OH)2
• CAS No.: 1174064-40-4
• Molecular Formula: C₁₃H₁₀BBr₂NO₃
• Molecular Weight: 398.846
• Mol file: 1174064-40-4.mol

Synonyms:

Chemical Property of HOC₆H₂Br₂CHNC₆H₄B(OH)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of HOC₆H₂Br₂CHNC₆H₄B(OH)2

There total 2 articles about HOC₆H₂Br₂CHNC₆H₄B(OH)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

3,5-Dibromosalicylaldehyde (90-59-5) + 3-Aminophenylboronic acid (30418-59-8,280563-63-5) → HOC6H2Br2CHNC6H4B(OH)2 (1174064-40-4)

Guidance literature:

In methanol; acetonitrile; at 20 ℃;

DOI:10.1016/j.jorganchem.2009.02.025

Reference yield: 65.0%

3,5-Dibromosalicylaldehyde (90-59-5) + 3-aminobenzeneboronic acid monohydrate (206658-89-1) → HOC6H2Br2CHNC6H4B(OH)2 (1174064-40-4)

Guidance literature:

In methanol; acetonitrile; mixt. of B compd. and aldehyde in MeOH/CH3CN was stirred at room temp. for 1 h; after 12 h filtered; dried (vac.);

DOI:10.1016/j.jorganchem.2009.02.025

upstream raw materials:

3,5-Dibromosalicylaldehyde

3-aminobenzeneboronic acid monohydrate

3-Aminophenylboronic acid