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(R)-Tetrahydro-2-furancarbothioic acid

Base Information Edit
  • Chemical Name:(R)-Tetrahydro-2-furancarbothioic acid
  • CAS No.:153165-72-1
  • Molecular Formula:C5H8O2S
  • Molecular Weight:132.183
  • Hs Code.:
  • UNII:7K6LJV2M2M
  • Mol file:153165-72-1.mol
(R)-Tetrahydro-2-furancarbothioic acid

Synonyms:(R)-Tetrahydro-2-furancarbothioic acid;153165-72-1;(2R)-oxolane-2-carbothioic S-acid;(2R)-OXOLANE-2-CARBOTHIOIC O-ACID;2-Furancarbothioic acid, tetrahydro-, (2R)-;(2R)-Tetrahydro-2-furancarbothioic acid;(R)-Tetrahydrofuran-2-carbothioic S-acid;7K6LJV2M2M;SCHEMBL6396574;VXYYXBQTPJTYOB-SCSAIBSYSA-N;AKOS015899805;(R)-Tetrahydrofuran-2-carbothioic O-acid;Tetrahydro-2-furancarbothioic acid, (R)-;(2R)-tetrahydrofuran-2-thiocarboxylic acid;2-Furancarbothioic acid tetrahydro-, (2R)-;2-Furancarbothioic acid, tetrahydro-, (R)-;R-(+)-Thio-terahydrofuran-2-carboxylic acid

Suppliers and Price of (R)-Tetrahydro-2-furancarbothioic acid
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • Labseeker
  • (R)-Tetrahydro-2-furancarbothioicacid 95
  • 100kg
  • $ 35000.00
Total 14 raw suppliers
Chemical Property of (R)-Tetrahydro-2-furancarbothioic acid Edit
Chemical Property:
  • Boiling Point:212.033 °C at 760 mmHg 
  • PKA:3.26±0.20(Predicted) 
  • Flash Point:119.68 °C 
  • PSA:65.10000 
  • Density:1.218 g/cm3 
  • LogP:0.62180 
  • XLogP3:0.7
  • Hydrogen Bond Donor Count:1
  • Hydrogen Bond Acceptor Count:3
  • Rotatable Bond Count:1
  • Exact Mass:132.02450067
  • Heavy Atom Count:8
  • Complexity:103
Purity/Quality:

99%, *data from raw suppliers

(R)-Tetrahydro-2-furancarbothioicacid 95 *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
  • Canonical SMILES:C1CC(OC1)C(=O)S
  • Isomeric SMILES:C1C[C@@H](OC1)C(=O)S
Technology Process of (R)-Tetrahydro-2-furancarbothioic acid

There total 1 articles about (R)-Tetrahydro-2-furancarbothioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dmap; 5-amino-3H-1,2,4-dithiazole-3-thione; In N,N-dimethyl-formamide; at 100 ℃; for 24h; Reagent/catalyst; Solvent; Green chemistry;
Guidance literature:
Multi-step reaction with 5 steps
1: aq. NaHCO3 / acetone / 4 h / 60 °C
2: Et3N / CH2Cl2 / 0.17 h / -20 °C
3: triethyl phosphite / xylene / 11 h / Heating
4: AcOH, tetra-n-butylammonium fluoride / tetrahydrofuran / 8.5 h / 50 °C
5: Ph3P, tetrakis(triphenylphosphine)palladium, potassium 2-ethylhexanoate / ethyl acetate / 1 h / Ambient temperature
With tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium 2-ethylhexanoate; acetic acid; triethylamine; triphenylphosphine; triethyl phosphite; In tetrahydrofuran; dichloromethane; ethyl acetate; acetone; xylene;
DOI:10.1016/S0968-0896(97)00073-4
Guidance literature:
Multi-step reaction with 6 steps
1: 90 percent / aq. NaHCO3 / acetone / 4 h / 60 °C
2: Et3N / CH2Cl2 / 0.17 h / -20 °C
3: triethyl phosphite / xylene / 11 h / Heating
4: 81 percent / AcOH, tetra-n-butylammonium fluoride / tetrahydrofuran / 8.5 h / 50 °C
5: 20 percent / ethyl acetate / Irradiation
6: 25 percent / Ph3P, tetrakis(triphenylphosphine)palladium, sodium 2-ethylhexanoate / ethyl acetate / 1 h / Ambient temperature
With tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; sodium hydrogencarbonate; acetic acid; triethylamine; triphenylphosphine; triethyl phosphite; sodium 2-ethylhexanoic acid; In tetrahydrofuran; dichloromethane; ethyl acetate; acetone; xylene;
DOI:10.1016/S0968-0896(97)00073-4
upstream raw materials:

(R)-tetrahydro-2-furoic acid

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