C₉H₁₁F₃N₂O*ClH

Base Information

Chemical Name:C₉H₁₁F₃N₂O*ClH
CAS No.:1294519-40-6
Molecular Formula:C₉H₁₁F₃N₂O*ClH
Molecular Weight:256.655
Hs Code.:

C<sub>9</sub>H<sub>11</sub>F<sub>3</sub>N<sub>2</sub>O*ClH

Synonyms:

Suppliers and Price of C₉H₁₁F₃N₂O*ClH

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of C₉H₁₁F₃N₂O*ClH

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of C₉H₁₁F₃N₂O*ClH

There total 8 articles about C₉H₁₁F₃N₂O*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 953780-32-0
(R)-2-methyl-N-[(1R)-(5-(2,2,2-trifluoroethoxy)pyridin-2-yl)ethyl]propane-2-sulfinamide

: 1294519-40-6,953780-72-8
C₉H₁₁F₃N₂O*ClH

Guidance literature:: With hydrogenchloride; In methanol; diethyl ether; at 20 ℃; for 0.25h;
DOI:10.1016/j.bmcl.2011.01.089

Reference yield:

: 1121-78-4
5-Hydroxy-2-methylpyridine

: 1294519-40-6,953780-72-8
C₉H₁₁F₃N₂O*ClH

Guidance literature:: Multi-step reaction with 8 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h

2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 20 °C

3.1: 1 h / 100 °C

4.1: methanol; potassium carbonate

5.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0.17 h / Cooling with ice

5.2: 0.5 h

6.1: copper(II) sulfate / dichloromethane / 14 h / 20 °C

7.1: dichloromethane / -78 °C

8.1: hydrogenchloride / methanol; diethyl ether / 0.25 h / 20 °C

With hydrogenchloride; methanol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; copper(II) sulfate; 3-chloro-benzenecarboperoxoic acid; potassium bromide; In methanol; diethyl ether; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.089

Reference yield:

: 864263-61-6
2-methyl-5-(2,2,2-trifluoroethoxy)pyridine

: 1294519-40-6,953780-72-8
C₉H₁₁F₃N₂O*ClH

Guidance literature:: Multi-step reaction with 7 steps

1.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 20 °C

2.1: 1 h / 100 °C

3.1: methanol; potassium carbonate

4.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0.17 h / Cooling with ice

4.2: 0.5 h

5.1: copper(II) sulfate / dichloromethane / 14 h / 20 °C

6.1: dichloromethane / -78 °C

7.1: hydrogenchloride / methanol; diethyl ether / 0.25 h / 20 °C

With hydrogenchloride; methanol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium carbonate; copper(II) sulfate; 3-chloro-benzenecarboperoxoic acid; potassium bromide; In methanol; diethyl ether; dichloromethane; chloroform; water;
DOI:10.1016/j.bmcl.2011.01.089