1-[2-(Bromomethyl)-1,3-dioxolan-2-yl]-N-(phenylmethyl)cyclopropanecarboxamide

Base Information

• Chemical Name: 1-[2-(Bromomethyl)-1,3-dioxolan-2-yl]-N-(phenylmethyl)cyclopropanecarboxamide
• CAS No.: 147011-41-4
• Molecular Formula: C15H18BrNO3
• Molecular Weight: 340.21
• Mol file: 147011-41-4.mol

Synonyms:1-Benzylaminocarbonyl-1-(2-bromo-1,1-ethylenedioxyethyl)cyclopropane;

Chemical Property of 1-[2-(Bromomethyl)-1,3-dioxolan-2-yl]-N-(phenylmethyl)cyclopropanecarboxamide

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.599
• Boiling Point: 509.861 °C at 760 mmHg
• Flash Point: 262.155 °C
• PSA: 51.05000
• Density: 1.481 g/cm³
• LogP: 3.06130

Purity/Quality:

97% ^*data from raw suppliers

1-[2-(Bromomethyl)-1,3-dioxolan-2-yl]-N-(phenylmethyl)cyclopropanecarboxamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[2-(Bromomethyl)-1,3-dioxolan-2-yl]-N-(phenylmethyl)cyclopropanecarboxamide

There total 1 articles about 1-[2-(Bromomethyl)-1,3-dioxolan-2-yl]-N-(phenylmethyl)cyclopropanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1-(1,1-ethylenedioxyethyl)-1-benzylamidecyclopropane (147011-40-3) → 1-(2-bromo-1,1-ethylenedioxyethyl)-1-benzylamidecyclopropane (147011-41-4)

Guidance literature:

With bromine; In 1,4-dioxane; diethyl ether; at 20 ℃; for 5h;

DOI:10.1002/ardp.200700060

Reference yield: 98.0%

1-(2-bromo-1,1-ethylenedioxyethyl)-1-benzylamidecyclopropane (147011-41-4) → 5-benzyl-7,7-ethylenedioxy-4-oxo-5-azaspiro[2.4]heptane (147011-42-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 2h;

DOI:10.1002/ardp.200700060

upstream raw materials:

1-(1,1-ethylenedioxyethyl)-1-benzylamidecyclopropane

Downstream raw materials:

5-benzyl-7,7-ethylenedioxy-4-oxo-5-azaspiro[2.4]heptane

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