Anthracene, 9-bromo-10-(1-naphthalenyl)-

Base Information

• Chemical Name: Anthracene, 9-bromo-10-(1-naphthalenyl)-
• CAS No.: 400607-04-7
• Molecular Formula: C24H15Br
• Molecular Weight: 383.287
• Hs Code.: 2903999090
• Mol file: 400607-04-7.mol

Synonyms:10-(Naphthalene-1-yl)-9-bromo anthracene;9-Bromo-10-(2-naphthyl)anthracene;9-Bromo-10-(naphthalen-1-yl)anthracene;9-Bromo-10-(1-naphthalenyl)anthracene;

Chemical Property of Anthracene, 9-bromo-10-(1-naphthalenyl)-

Chemical Property:

• Appearance/Colour: Yellow powder
• Melting Point: 177.0 to 181.0 °C
• Refractive Index: 1.756
• Boiling Point: 508 °C at 760 mmHg
• Flash Point: 254.3 °C
• PSA: 0.00000
• Density: 1.403 g/cm³
• LogP: 7.57570
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: soluble in Toluene

Purity/Quality:

99% ^*data from raw suppliers

9-Bromo-10-(naphthalen-1-yl)anthracene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Anthracene, 9-bromo-10-(1-naphthalenyl)-

There total 7 articles about Anthracene, 9-bromo-10-(1-naphthalenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

10-(naphthalen-1-yl)anthracene (7424-70-6) → 10-bromo-9-(naphthalene-1'-yl)anthracene (400607-04-7)

Guidance literature:

With N-Bromosuccinimide; In chloroform; at 60 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c1jm14482k

Reference yield: 90.0%

→ 10-bromo-9-(naphthalene-1'-yl)anthracene (400607-04-7)

Guidance literature:

With N-Bromosuccinimide; In chloroform; at 80 ℃; for 12h;

Reference yield: 80.0%

9,10-Dibromoanthracene (523-27-3) + 1-Naphthylboronic acid (13922-41-3) → 10-bromo-9-(naphthalene-1'-yl)anthracene (400607-04-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 80 ℃; for 2h;

upstream raw materials:

9,10-Dibromoanthracene

1-Naphthylboronic acid

9-Bromoanthracene

10-(naphthalen-1-yl)anthracene

Downstream raw materials:

4,4,5,5-tetramethyl-2-(10-naphthalene-1-yl-anthracene-9-yl)-[1,3,2]dioxaborolane

C₃₇H₂₃N

9-(9-phenylcarbazole-3-yl)-10-(naphthalene-1-yl)anthracene

Refernces

• 1、 -. "Organic compound and electronic element and electronic device using same (by machine translation)". Paragraph 0140-0143; 0146. . Retrieved 2021/01/15.
• 2、 -. "Blue light electroluminescent material and application thereof". . . Retrieved 2020/01/25.