(E)-2-(3-methylstyryl)naphthalene

Base Information

Chemical Name:(E)-2-(3-methylstyryl)naphthalene
CAS No.:38503-47-8
Molecular Formula:C₁₉H₁₆
Molecular Weight:244.336
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(3-methylstyryl)naphthalene

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Technology Process of (E)-2-(3-methylstyryl)naphthalene

There total 7 articles about (E)-2-(3-methylstyryl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2947-60-6
3-methylbenzyl cyanide

2,2-dimethylpropanoic acid 2-naphthalenylmethyl ester: 2,2-dimethylpropanoic acid 2-naphthalenylmethyl ester

: 38503-47-8,93371-10-9
(E)-2-(3-methylstyryl)naphthalene

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,3-bis-(diphenylphosphino)propane; potassium tert-butylate; In 1,4-dioxane; at 100 ℃; stereoselective reaction; Inert atmosphere; Glovebox; Schlenk technique; Sealed tube;
DOI:10.1039/c5cc10005d

Reference yield: 53.0%

: 59305-33-8
[(m-tolylmethylene)bis(trimethylsilane)]

: 75472-75-2
(E)-N-((naphthalen-6-yl)methylene)benzenamine

: 38503-47-8,93371-10-9
(E)-2-(3-methylstyryl)naphthalene

Guidance literature:: With cesium fluoride; In N,N-dimethyl-formamide; at 80 ℃; for 4h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201500475

Reference yield:

: 35160-95-3
(2-naphthalenylmethyl)triphenylphosphonium bromide

: 620-22-4
3-Methylbenzonitrile

: 38503-47-8,93371-10-9
(E)-2-(3-methylstyryl)naphthalene

: 2-(3-methylstyryl)naphthalene

Guidance literature:: 3-Methylbenzonitrile; With diisobutylaluminium hydride; In hexane; dichloromethane; at -80 - 0 ℃; for 2.16667h;

(2-naphthalenylmethyl)triphenylphosphonium bromide; With lithium hydroxide monohydrate; In isopropyl alcohol; for 3h; Overall yield = 75%; Overall yield = 458.3 mg; Reflux;
DOI:10.1021/acs.joc.6b01450