C₁₅H₁₄ClNO₃S

Base Information

• Chemical Name: C₁₅H₁₄ClNO₃S
• CAS No.: 867356-97-6
• Molecular Formula: C₁₅H₁₄ClNO₃S
• Molecular Weight: 323.8
• Mol file: 867356-97-6.mol

Synonyms:

Chemical Property of C₁₅H₁₄ClNO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₄ClNO₃S

There total 6 articles about C₁₅H₁₄ClNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H14ClNO2S (1393639-50-3) → C15H14ClNO3S (867356-97-6)

Guidance literature:

With dihydrogen peroxide; acetic acid; at 20 ℃;

DOI:10.1016/j.ejmech.2012.05.038

Reference yield:

C15H13ClO3S (1393639-43-4) → C15H14ClNO3S (867356-97-6)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride

2: ammonium hydroxide / methanol / 20 °C

3: dihydrogen peroxide; acetic acid / 20 °C

With ammonium hydroxide; thionyl chloride; dihydrogen peroxide; acetic acid; In methanol;

DOI:10.1016/j.ejmech.2012.05.038

Reference yield:

2-Fluorobenzaldehyde (446-52-6) → C15H14ClNO3S (867356-97-6)

Guidance literature:

Multi-step reaction with 7 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / Reflux

2.1: sodium tetrahydroborate; isopropyl alcohol / 20 °C

3.1: hydrogen bromide / water / 0.5 h / Reflux

4.1: sodium hydroxide / 1 h / 80 °C

4.2: 2 h / Reflux

5.1: thionyl chloride

6.1: ammonium hydroxide / methanol / 20 °C

7.1: dihydrogen peroxide; acetic acid / 20 °C

With ammonium hydroxide; sodium tetrahydroborate; thionyl chloride; hydrogen bromide; dihydrogen peroxide; caesium carbonate; acetic acid; isopropyl alcohol; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.05.038

upstream raw materials:

C₁₅H₁₄ClNO₂S

C₁₅H₁₃ClO₃S

C₁₄H₁₃ClN₂OS

4-chloro-phenol