E-4-coumaroyllupinine

Base Information

• Chemical Name: E-4-coumaroyllupinine
• CAS No.: 58548-44-0
• Molecular Formula: C₁₉H₂₅NO₃
• Molecular Weight: 315.412
• Mol file: 58548-44-0.mol

Synonyms:

Chemical Property of E-4-coumaroyllupinine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of E-4-coumaroyllupinine

There total 4 articles about E-4-coumaroyllupinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-Coumaric Acid (7400-08-0,50940-26-6) → E-4-coumaroyllupinine (58548-44-0,71635-27-3,88644-37-5,132295-18-2)

Guidance literature:

Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimid

2: NaHCO₃ / acetone; H₂O / 12 h

3: hydroxycinnamoyl-CoA:13-lupinine-O-hydroxycinnamoyltransferase from Lupinus luteus / 0.33 h / 37 °C / buffer; pH=7.0

With sodium hydrogencarbonate; dicyclohexyl-carbodiimide; hydroxycinnamoyl-CoA:13-lupinine-O-hydroxycinnamoyltransferase from Lupinus luteus; In water; acetone;

DOI:10.1016/0031-9422(91)84195-X

Reference yield:

4-hydroxycinnamic acid N-hydroxysuccinimide ester (88492-43-7) → E-4-coumaroyllupinine (58548-44-0,71635-27-3,88644-37-5,132295-18-2)

Guidance literature:

Multi-step reaction with 2 steps

1: NaHCO₃ / acetone; H₂O / 12 h

2: hydroxycinnamoyl-CoA:13-lupinine-O-hydroxycinnamoyltransferase from Lupinus luteus / 0.33 h / 37 °C / buffer; pH=7.0

With sodium hydrogencarbonate; hydroxycinnamoyl-CoA:13-lupinine-O-hydroxycinnamoyltransferase from Lupinus luteus; In water; acetone;

DOI:10.1016/0031-9422(91)84195-X

Reference yield:

lupinine (10159-79-2) + hydroxycinnamoyl-S-CoA (30802-00-7,119785-99-8) → E-4-coumaroyllupinine (58548-44-0,71635-27-3,88644-37-5,132295-18-2)

Guidance literature:

hydroxycinnamoyl-CoA:13-lupinine-O-hydroxycinnamoyltransferase from Lupinus luteus; at 37 ℃; for 0.333333h; buffer; pH=7.0;

DOI:10.1016/0031-9422(91)84195-X

upstream raw materials:

lupinine

hydroxycinnamoyl-S-CoA

p-Coumaric Acid

4-hydroxycinnamic acid N-hydroxysuccinimide ester