2-(2-thienyl)-5--1,3-oxazoline hydrochloride

Base Information

Chemical Name:2-(2-thienyl)-5--1,3-oxazoline hydrochloride
CAS No.:120123-65-1
Molecular Formula:C₁₆H₁₆ClFN₂OS*ClH
Molecular Weight:375.294
Hs Code.:

2-(2-thienyl)-5-<N-(3-fluorophenyl)-N-(2-chloroethyl)-aminomethyl>-1,3-oxazoline hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-thienyl)-5--1,3-oxazoline hydrochloride

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Technology Process of 2-(2-thienyl)-5--1,3-oxazoline hydrochloride

There total 1 articles about 2-(2-thienyl)-5--1,3-oxazoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120106-79-8
Thiophene-2-carboxylic acid {3-[(3-fluoro-phenyl)-(2-hydroxy-ethyl)-amino]-2-hydroxy-propyl}-amide

: 120106-82-3
N₁-(3-fluorophenyl)-N₁-(2-chloroethyl)-N₂-(2-thienylcarbonyl)-2-chloro-1,3-diaminopropane

: 120123-65-1
2-(2-thienyl)-5--1,3-oxazoline hydrochloride

Guidance literature:: With thionyl chloride; In dichloromethane; for 0.75h; Yield given; Heating;
DOI:10.1016/0223-5234(88)90007-4

Reference yield:

: 120123-65-1
2-(2-thienyl)-5--1,3-oxazoline hydrochloride

: 96306-34-2,105138-32-7,120106-97-0,120106-98-1
(+)-10-fluoro-1,2,3,4,4a,5-hexahydro-3-methyl-7-(2-thienyl)-pyrazino<1,2-a><1,4>benzodiazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 5 percent / POCl₃, H₂O

2: 41.7 percent / (-)-O,O'-dibenzoyl-L-tartaric acid, 2.) NaOH / CH₂Cl₂

3: 65.2 percent / methanol; H₂O / 14 h / 90 °C / autoclave

With sodium hydroxide; water; (-)-Dibenzoyl-L-tartaric acid; trichlorophosphate; In methanol; dichloromethane; water;
DOI:10.1016/0223-5234(88)90007-4

Reference yield:

: 120123-65-1
2-(2-thienyl)-5--1,3-oxazoline hydrochloride

: 96306-34-2,120106-97-0,120106-98-1
10-fluoro-1,2,3,4,4a,5-hexahydro-3-methyl-7-(2-thienyl)-pyrazino[1,2-a][1,4]benzodiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 5 percent / POCl₃, H₂O

2: 68 percent / H₂O; methanol / 14 h / 90 °C / autoclave

With water; trichlorophosphate; In methanol; water;
DOI:10.1016/0223-5234(88)90007-4