C₄₁H₃₃F₃N₄O

Base Information

Chemical Name:C₄₁H₃₃F₃N₄O
CAS No.:1629023-80-8
Molecular Formula:C₄₁H₃₃F₃N₄O
Molecular Weight:654.734
Hs Code.:

C<sub>41</sub>H<sub>33</sub>F<sub>3</sub>N<sub>4</sub>O

Synonyms:

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Chemical Property of C₄₁H₃₃F₃N₄O

Chemical Property:

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Technology Process of C₄₁H₃₃F₃N₄O

There total 12 articles about C₄₁H₃₃F₃N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620327-60-7
C₃₂H₂₉BF₃N₃O₂

: 1629023-35-3
C₁₅H₁₆BrNO

: 1629023-80-8
C₄₁H₃₃F₃N₄O

Guidance literature:: With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; water; at 20 ℃; for 2.5h;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 1160502-31-7
4-iodo-3-(trifluoromethyl)-1-tritylpyrazolo[5,4-b]pyridine

: 1629023-80-8
C₄₁H₃₃F₃N₄O

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 14 h / 105 °C

2: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 2.5 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium acetate; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; water; N,N-dimethyl-formamide; 1: |Suzuki Coupling / 2: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 1435-51-4
1,3-dibromo-5-fluorobenzene

: 1629023-80-8
C₄₁H₃₃F₃N₄O

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / 1-methyl-pyrrolidin-2-one / 24 h / 120 °C

2.1: lithium chloride / dimethyl sulfoxide; water / 3 h / 165 °C

3.1: tetrabutylammomium bromide; sodium hydroxide / toluene; water / 16 h / 20 °C

4.1: copper(l) cyanide; TurboGrignard / tetrahydrofuran / 1 h / 0 - 20 °C

5.1: ozone / dichloromethane; methanol / 1 h / -78 °C

5.2: 16 h / -78 - 20 °C

6.1: tetrahydrofuran / 16 h / -78 - 20 °C

7.1: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 2.5 h / 20 °C

With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; TurboGrignard; tetrabutylammomium bromide; copper(l) cyanide; sodium hydride; ozone; lithium chloride; sodium hydroxide; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; 2.1: |Krapcho Dealkoxycarbonylation / 6.1: |Grignard Reaction / 7.1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.05.082