[RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]⁽¹⁺⁾*SbF₆^(1-)=[RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]SbF₆

Base Information

• Chemical Name: [RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]⁽¹⁺⁾*SbF₆^(1-)=[RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]SbF₆
• CAS No.: 1046476-58-7
• Molecular Formula: C₂₄H₃₆ClN₂Ru*F₆Sb
• Molecular Weight: 724.827
• Mol file: 1046476-58-7.mol

Synonyms:

Chemical Property of [RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]⁽¹⁺⁾*SbF₆^(1-)=[RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]SbF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]⁽¹⁺⁾*SbF₆^(1-)=[RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]SbF₆

There total 1 articles about [RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]⁽¹⁺⁾*SbF₆^(1-)=[RuCl(CH₃C₆H₄CH(CH₃)2)(C₆H₁₁CH(CH₃)NHCH₂C₅H₄N)]SbF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium hexafluoroantimonate (16925-25-0) + [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) + (R)-C5H4NCH2NHCH(Me)Cy (103382-80-5) → [RuCl(CH3C6H4CH(CH3)2)(C6H11CH(CH3)NHCH2C5H4N)](1+)*SbF6(1-)=[RuCl(CH3C6H4CH(CH3)2)(C6H11CH(CH3)NHCH2C5H4N)]SbF6 (1046476-58-7)

Guidance literature:

In methanol; mixt. was stirred in solvent for 14 h; ppt. was filtered, recrystd. from CH2Cl2-Et2O, filtrate was evapd. in vac. to dryness, residue was extd. with CH2Cl2 and concd. under reduced pressure, slow addition of Et2O dive solids, ppt. was filtered off, washedwith Et2O, dried in air; elem. anal.;

DOI:10.1039/b802381f

Reference yield: 70.0%

[RuCl(CH3C6H4CH(CH3)2)(C6H11CH(CH3)NHCH2C5H4N)](1+)*SbF6(1-)=[RuCl(CH3C6H4CH(CH3)2)(C6H11CH(CH3)NHCH2C5H4N)]SbF6 (1046476-58-7) + water (7732-18-5) → [RuH2O(CH3C6H4CH(CH3)2)(C6H11CH(CH3)NHCH2C5H4N)](2+)*2SbF6(1-)=[RuH2O(CH3C6H4CH(CH3)2)(C6H11CH(CH3)NHCH2C5H4N)](SbF6)2

Guidance literature:

With AgSbF₆; In dichloromethane; acetone; byproducts: AgCl; to mixt. of complexes in CH2Cl2 was added AgSbF6 in acetone, suspn. stirred for 30 min; ppt. was filtered off, soln. was evapd. in vac. to dryness, Et2O added with vigorous stirring; elem. anal.;

DOI:10.1039/b802381f

upstream raw materials:

sodium hexafluoroantimonate

[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

(R)-C₅H₄NCH₂NHCH(Me)Cy