barbatolin

Base Information

Chemical Name:barbatolin
CAS No.:114973-13-6
Molecular Formula:C₁₇H₁₄O₈
Molecular Weight:346.293
Hs Code.:

Synonyms:

Suppliers and Price of barbatolin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of barbatolin

Chemical Property:

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Technology Process of barbatolin

There total 6 articles about barbatolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 114973-12-5
4-bromomethyl-2,6-dihydroxybenzaldehyde

: 114973-10-3
potassium haematommate

: 114973-13-6
barbatolin

Guidance literature:: In N,N-dimethyl acetamide; for 12h; Ambient temperature;

Reference yield:

: 705-76-0
3,5-dimethoxybenzyl alcohol

: 114973-13-6
barbatolin

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride / 1.) dimethyl sulfoxide, 1 h, 2.) dimethyl sulfoxide, RT, 1 h

2: 1.) phenyllithium / 1.) ether, RT, 24 h, 2.) ether, RT, 1.5 h

3: 68 percent / boron tribromide / 1.) -78 deg C, 0.5 h, 2.) RT, 0.5 h

4: 29 percent / N,N-dimethyl-acetamide / 12 h / Ambient temperature

With boron tribromide; sodium hydride; phenyllithium; In N,N-dimethyl acetamide;

Reference yield:

: 73569-69-4
1-methylmethoxy-3,5-dimethoxybenzene

: 114973-13-6
barbatolin

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) phenyllithium / 1.) ether, RT, 24 h, 2.) ether, RT, 1.5 h

2: 68 percent / boron tribromide / 1.) -78 deg C, 0.5 h, 2.) RT, 0.5 h

3: 29 percent / N,N-dimethyl-acetamide / 12 h / Ambient temperature

With boron tribromide; phenyllithium; In N,N-dimethyl acetamide;