C₂₂H₂₀BrF₂N₃O₃

Base Information

Chemical Name:C₂₂H₂₀BrF₂N₃O₃
CAS No.:736925-05-6
Molecular Formula:C₂₂H₂₀BrF₂N₃O₃
Molecular Weight:492.32
Hs Code.:

C<sub>22</sub>H<sub>20</sub>BrF<sub>2</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₂H₂₀BrF₂N₃O₃

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Technology Process of C₂₂H₂₀BrF₂N₃O₃

There total 8 articles about C₂₂H₂₀BrF₂N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 675-10-5
4-hydroxy-6-methyl-2-pyron

: 736925-05-6
C₂₂H₂₀BrF₂N₃O₃

Guidance literature:: Multi-step reaction with 7 steps

1: water / 48 h / 100 °C

2: caesium carbonate / acetone / 25 °C

3: 4-methyl-morpholine; 1,3,5-trichloro-2,4,6-triazine / dichloromethane; N,N-dimethyl-formamide / 2 h

4: ammonia / methanol / 24 h / 20 °C

5: N-Bromosuccinimide / acetonitrile / 0 - 25 °C

6: 4-methyl-morpholine; benzotriazol-1-ol / dichloromethane; N,N-dimethyl acetamide / 4 h / 20 °C

7: hydrogenchloride / 1,4-dioxane

With 4-methyl-morpholine; hydrogenchloride; N-Bromosuccinimide; 1,3,5-trichloro-2,4,6-triazine; ammonia; benzotriazol-1-ol; caesium carbonate; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2011.04.120

Reference yield:

: 586376-24-1
C₂₀H₁₆ClF₂NO₂

: 736925-05-6
C₂₂H₂₀BrF₂N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1: ammonia / methanol / 24 h / 20 °C

2: N-Bromosuccinimide / acetonitrile / 0 - 25 °C

3: 4-methyl-morpholine; benzotriazol-1-ol / dichloromethane; N,N-dimethyl acetamide / 4 h / 20 °C

4: hydrogenchloride / 1,4-dioxane

With 4-methyl-morpholine; hydrogenchloride; N-Bromosuccinimide; ammonia; benzotriazol-1-ol; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl acetamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.04.120

Reference yield:

: 586375-19-1
1-[3-(hydroxymethyl)phenyl]-4-[(2,4-difluorobenzyl)oxy]-6-methylpyridin-2(1H)-one

: 736925-05-6
C₂₂H₂₀BrF₂N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1: 4-methyl-morpholine; 1,3,5-trichloro-2,4,6-triazine / dichloromethane; N,N-dimethyl-formamide / 2 h

2: ammonia / methanol / 24 h / 20 °C

3: N-Bromosuccinimide / acetonitrile / 0 - 25 °C

4: 4-methyl-morpholine; benzotriazol-1-ol / dichloromethane; N,N-dimethyl acetamide / 4 h / 20 °C

5: hydrogenchloride / 1,4-dioxane

With 4-methyl-morpholine; hydrogenchloride; N-Bromosuccinimide; 1,3,5-trichloro-2,4,6-triazine; ammonia; benzotriazol-1-ol; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.04.120