4-Acetylphenanthrene

Base Information

• Chemical Name: 4-Acetylphenanthrene
• CAS No.: 26698-33-9
• Molecular Formula: C₁₆H₁₂O
• Molecular Weight: 220.271
• Mol file: 26698-33-9.mol

Synonyms:

Chemical Property of 4-Acetylphenanthrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Acetylphenanthrene

There total 3 articles about 4-Acetylphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-acetyl-phenanthrene-3-carboxylic acid → 4-acetylphenantrene (26698-33-9)

Guidance literature:

With quinoline; copper (II) carbonate hydroxide; at 240 - 260 ℃;

DOI:10.1021/ja01302a069

Reference yield:

2-(Phenanthrene-4-carbonyl)-malonic acid diethyl ester (26698-30-6) → 4-acetylphenantrene (26698-33-9)

Guidance literature:

Multistep reaction; (i) (hydrolysis), (ii) (decarboxylation);

DOI:10.1021/jm00296a016

Reference yield:

→ 4-acetylphenantrene (26698-33-9)

Guidance literature:

aus Photolyse von 3-Acetyl-stilben;

upstream raw materials:

2-(Phenanthrene-4-carbonyl)-malonic acid diethyl ester