trifluoro-methanesulfonic acid 7-benzyloxy-4-[2-(tert-butyl-diphenyl-silanyloxy)-1-formyl-ethyl]-3-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

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Chemical Name:trifluoro-methanesulfonic acid 7-benzyloxy-4-[2-(tert-butyl-diphenyl-silanyloxy)-1-formyl-ethyl]-3-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester
CAS No.:925463-52-1
Molecular Formula:C₅₉H₆₀F₃NO₉S₂Si₂
Molecular Weight:1104.42
Hs Code.:

trifluoro-methanesulfonic acid 7-benzyloxy-4-[2-(<i>tert</i>-butyl-diphenyl-silanyloxy)-1-formyl-ethyl]-3-(<i>tert</i>-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1<i>H</i>-indol-5-yl ester

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Chemical Property of trifluoro-methanesulfonic acid 7-benzyloxy-4-[2-(tert-butyl-diphenyl-silanyloxy)-1-formyl-ethyl]-3-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

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Technology Process of trifluoro-methanesulfonic acid 7-benzyloxy-4-[2-(tert-butyl-diphenyl-silanyloxy)-1-formyl-ethyl]-3-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

There total 2 articles about trifluoro-methanesulfonic acid 7-benzyloxy-4-[2-(tert-butyl-diphenyl-silanyloxy)-1-formyl-ethyl]-3-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trifluoro-methanesulfonic acid 5-benzyloxy-2,3-bis-[2-(tert-butyl-diphenyl-silanyloxy)-1-formyl-ethyl]-4-(toluene-4-sulfonylamino)-phenyl ester

: 925463-52-1
trifluoro-methanesulfonic acid 7-benzyloxy-4-[2-(tert-butyl-diphenyl-silanyloxy)-1-formyl-ethyl]-3-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

Guidance literature:: With sulfuric acid; In tetrahydrofuran;
DOI:10.1021/jo062064j

Reference yield:

: trifluoro-methanesulfonic acid 3-benzyloxy-5,8-bis-(tert-butyl-diphenyl-silanyloxymethyl)-6,7-dihydroxy-4-(toluene-4-sulfonylamino)-5,6,7,8-tetrahydro-naphthalen-1-yl ester

: 925463-52-1
trifluoro-methanesulfonic acid 7-benzyloxy-4-[2-(tert-butyl-diphenyl-silanyloxy)-1-formyl-ethyl]-3-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium periodate on silica gel / CH₂Cl₂ / 1 h

2: 0.214 g / sulfuric acid / tetrahydrofuran

With sodium periodate; sulfuric acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo062064j