2-(4'-diethylsulfonamide phenyl)-1,3,4-oxadiazolin-5-thione

Base Information

Chemical Name:2-(4'-diethylsulfonamide phenyl)-1,3,4-oxadiazolin-5-thione
CAS No.:552305-10-9
Molecular Formula:C₁₂H₁₅N₃O₃S₂
Molecular Weight:313.401
Hs Code.:

Synonyms:

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Chemical Property of 2-(4'-diethylsulfonamide phenyl)-1,3,4-oxadiazolin-5-thione

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Technology Process of 2-(4'-diethylsulfonamide phenyl)-1,3,4-oxadiazolin-5-thione

There total 4 articles about 2-(4'-diethylsulfonamide phenyl)-1,3,4-oxadiazolin-5-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 75-15-0,12122-00-8
carbon disulfide

: 53554-97-5
4-<(Diethylamino)sulfonyl>benzoic Acid Hydrazide

: 552305-10-9
2-(4'-diethylsulfonamide phenyl)-1,3,4-oxadiazolin-5-thione

Guidance literature:: With potassium hydroxide; In ethanol; for 8h; Heating;
DOI:10.1515/HC.2006.12.6.453

Reference yield:

: 951213-47-1
methyl 4-(N,N-diethylsulfamoyl)benzoate

: 552305-10-9
2-(4'-diethylsulfonamide phenyl)-1,3,4-oxadiazolin-5-thione

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / hydrazine hydrate / ethanol / 8 h / Heating

2: 68 percent / potassium hydroxide / ethanol / 8 h / Heating

With potassium hydroxide; hydrazine hydrate; In ethanol;
DOI:10.1515/HC.2006.12.6.453

Reference yield:

: 10130-89-9
p-carboxyphenylsulfonyl chloride

: 552305-10-9
2-(4'-diethylsulfonamide phenyl)-1,3,4-oxadiazolin-5-thione

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / NaOH / H₂O / 3 h / 30 °C

2: 83 percent / sulfuric acid / Heating

3: 75 percent / hydrazine hydrate / ethanol / 8 h / Heating

4: 68 percent / potassium hydroxide / ethanol / 8 h / Heating

With potassium hydroxide; sodium hydroxide; sulfuric acid; hydrazine hydrate; In ethanol; water;
DOI:10.1515/HC.2006.12.6.453