1-t-butyl 5-methyl (1'R,2R,5R)-2-(t-butyl)-3-methyl-5-<3'-oxo-1',4',4',4'-tetraphenylbutyl>-1,5-imidazolidinedicarboxylate

Base Information

Chemical Name:1-t-butyl 5-methyl (1'R,2R,5R)-2-(t-butyl)-3-methyl-5-<3'-oxo-1',4',4',4'-tetraphenylbutyl>-1,5-imidazolidinedicarboxylate
CAS No.:143430-72-2
Molecular Formula:C₄₃H₅₀N₂O₅
Molecular Weight:674.88
Hs Code.:

Synonyms:

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Chemical Property of 1-t-butyl 5-methyl (1'R,2R,5R)-2-(t-butyl)-3-methyl-5-<3'-oxo-1',4',4',4'-tetraphenylbutyl>-1,5-imidazolidinedicarboxylate

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Technology Process of 1-t-butyl 5-methyl (1'R,2R,5R)-2-(t-butyl)-3-methyl-5-<3'-oxo-1',4',4',4'-tetraphenylbutyl>-1,5-imidazolidinedicarboxylate

There total 4 articles about 1-t-butyl 5-methyl (1'R,2R,5R)-2-(t-butyl)-3-methyl-5-<3'-oxo-1',4',4',4'-tetraphenylbutyl>-1,5-imidazolidinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 143430-72-2
1-t-butyl 5-methyl (1'R,2R,5R)-2-(t-butyl)-3-methyl-5-<3'-oxo-1',4',4',4'-tetraphenylbutyl>-1,5-imidazolidinedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-butyllithium / 1) THF, hexane, 4 deg C, 1 h

2: 65 percent / chromium(VI)oxide, sat. sulfuric acid / acetone; H₂O

3: 1) DIPA, n-butyllithium / 1a) THF, hexane, -50 deg C, 20 min, 1b) -60 deg C, 35 min, 2) up to -40 deg C, 3.5 h

With chromium(VI) oxide; n-butyllithium; sulfuric acid; diisopropylamine; In water; acetone;

Reference yield:

: 519-73-3
triphenylmethane

: 143430-72-2
1-t-butyl 5-methyl (1'R,2R,5R)-2-(t-butyl)-3-methyl-5-<3'-oxo-1',4',4',4'-tetraphenylbutyl>-1,5-imidazolidinedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-butyllithium / 1) THF, hexane, 4 deg C, 1 h

2: 65 percent / chromium(VI)oxide, sat. sulfuric acid / acetone; H₂O

3: 1) DIPA, n-butyllithium / 1a) THF, hexane, -50 deg C, 20 min, 1b) -60 deg C, 35 min, 2) up to -40 deg C, 3.5 h

With chromium(VI) oxide; n-butyllithium; sulfuric acid; diisopropylamine; In water; acetone;

Reference yield:

: 97991-00-9
(E)-1,1,1,4-Tetraphenyl-3-buten-2-ol

: 143430-72-2
1-t-butyl 5-methyl (1'R,2R,5R)-2-(t-butyl)-3-methyl-5-<3'-oxo-1',4',4',4'-tetraphenylbutyl>-1,5-imidazolidinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / chromium(VI)oxide, sat. sulfuric acid / acetone; H₂O

2: 1) DIPA, n-butyllithium / 1a) THF, hexane, -50 deg C, 20 min, 1b) -60 deg C, 35 min, 2) up to -40 deg C, 3.5 h

With chromium(VI) oxide; n-butyllithium; sulfuric acid; diisopropylamine; In water; acetone;