Fmoc-Asp(OBzl)-OTcp

Base Information

• Chemical Name: Fmoc-Asp(OBzl)-OTcp
• CAS No.: 133478-40-7
• Molecular Formula: C₃₂H₂₄Cl₃NO₆
• Molecular Weight: 624.905
• Mol file: 133478-40-7.mol

Synonyms:

Chemical Property of Fmoc-Asp(OBzl)-OTcp

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Fmoc-Asp(OBzl)-OTcp

There total 2 articles about Fmoc-Asp(OBzl)-OTcp which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

9-fluorenylmethoxycarbonyl-O-benzyl-L-aspartic acid (150009-58-8,86060-84-6) + 2,4,5-trichlorophenol (95-95-4) → Fmoc-Asp(OBzl)-OTcp (133478-40-7)

Guidance literature:

With dicyclohexyl-carbodiimide;

Reference yield:

→ 2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-benzyl ester 1-(2,4,5-trichloro-phenyl) ester (133478-40-7)

Guidance literature:

aus FMOC-L-Asparaginsaeure-β-benzylester u. 2.4.5-Trichlorphenol;

DOI:10.1021/jo01334a038

upstream raw materials:

9-fluorenylmethoxycarbonyl-O-benzyl-L-aspartic acid

2,4,5-trichlorophenol

Refernces