2-tert-Butyl-4-phenyl-8a-perhydrochromenylphosphonic acid

Base Information

Chemical Name:2-tert-Butyl-4-phenyl-8a-perhydrochromenylphosphonic acid
CAS No.:138568-57-7
Molecular Formula:C₁₉H₂₉O₄P
Molecular Weight:352.411
Hs Code.:

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Chemical Property of 2-tert-Butyl-4-phenyl-8a-perhydrochromenylphosphonic acid

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Technology Process of 2-tert-Butyl-4-phenyl-8a-perhydrochromenylphosphonic acid

There total 3 articles about 2-tert-Butyl-4-phenyl-8a-perhydrochromenylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 138568-49-7
[2-(4,4-Dimethyl-3-oxo-1-phenyl-pentyl)-1-hydroxy-cyclohexyl]-phosphinic acid

: 138568-57-7
2-tert-Butyl-4-phenyl-8a-perhydrochromenylphosphonic acid

Guidance literature:: With acetic acid; for 40h; Heating;

Reference yield:

: 78530-95-7
4,4-dimethyl-1-phenyl-1-(2'-oxocyclohexyl)-3-pentanone

: 138568-57-7
2-tert-Butyl-4-phenyl-8a-perhydrochromenylphosphonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 2) water / 1) dioxane, 1 h, 2) 10 deg C

2: 72 percent / MeOH, water / 96 h / Ambient temperature

3: 94 percent / gl. AcOH / 40 h / Heating

With methanol; water; acetic acid;

Reference yield:

: 138568-47-5
[2-(4,4-Dimethyl-3-oxo-1-phenyl-pentyl)-1-trimethylsilanyloxy-cyclohexyl]-phosphinic acid

: 138568-57-7
2-tert-Butyl-4-phenyl-8a-perhydrochromenylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / MeOH, water / 96 h / Ambient temperature

2: 94 percent / gl. AcOH / 40 h / Heating

With methanol; water; acetic acid;