1,1,2,2-Tetrafluordiphenyldisilan

Base Information

Chemical Name:1,1,2,2-Tetrafluordiphenyldisilan
CAS No.:104925-66-8
Molecular Formula:C₁₂H₁₀F₄Si₂
Molecular Weight:286.376
Hs Code.:

Synonyms:

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Chemical Property of 1,1,2,2-Tetrafluordiphenyldisilan

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Technology Process of 1,1,2,2-Tetrafluordiphenyldisilan

There total 1 articles about 1,1,2,2-Tetrafluordiphenyldisilan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 43081-37-4
1,2-diphenyl-1,1,2,2-tetrachlorodisilane

: 104925-66-8
1,1,2,2-Tetrafluordiphenyldisilan

Guidance literature:: With zinc(II) fluoride; silver; at 65 ℃; for 12h;
DOI:10.1016/0022-328X(86)84027-X

Reference yield: 90.0%

: 126009-36-7
{Pd(styrene)(PMe₃)2}

: 104925-66-8
1,1,2,2-Tetrafluordiphenyldisilan

: 157261-55-7
trans-Pd(SiF₂Ph)2(PMe₃)2

Guidance literature:: In toluene; under N2; to soln. Pd-complex (generated in situ from trans-PdEt2(PMe3)2 and styrene in toluene) cooled to -20°C was added soln. of 3 equiv of the silane/toluene, soln. stirred (room temp., 1 h); evapn. (by pumping), solid dissolved in CH2Cl2 at room temp., layered with Et2O, kept at -70°C (crystn.), elem. anal.;
DOI:10.1021/om00020a042

Reference yield: 86.0%

: 137515-74-3
Pd(styrene)(PMe₂Ph)2

: 104925-66-8
1,1,2,2-Tetrafluordiphenyldisilan

: 157261-56-8
trans-Pd(SiF₂Ph)2(PMe₂Ph)2

Guidance literature:: In toluene; under N2; to soln. Pd-complex (generated in situ from trans-PdEt2(PMe2Ph)2 and styrene in toluene) cooled to -20°C was added soln. of 3 equiv of the silane/toluene, soln. stirred (room temp., 1 h); evapn. (by pumping), solid dissolved in CH2Cl2 at room temp., layered with Et2O, kept at -70°C (crystn.), elem. anal.;
DOI:10.1021/om00020a042