2,6-Dimethoxy-3-nitro-4-thiocyanophenyl acetate

Base Information

Chemical Name:2,6-Dimethoxy-3-nitro-4-thiocyanophenyl acetate
CAS No.:150563-52-3
Molecular Formula:C₁₁H₁₀N₂O₆S
Molecular Weight:298.276
Hs Code.:

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Chemical Property of 2,6-Dimethoxy-3-nitro-4-thiocyanophenyl acetate

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Technology Process of 2,6-Dimethoxy-3-nitro-4-thiocyanophenyl acetate

There total 3 articles about 2,6-Dimethoxy-3-nitro-4-thiocyanophenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 150563-51-2
2,6-Dimethoxy-4-thiocyanophenyl acetate

: 150563-52-3
2,6-Dimethoxy-3-nitro-4-thiocyanophenyl acetate

Guidance literature:: With nitric acid; In acetic anhydride; 0 deg C to room temp. then room temp., 1 h;
DOI:10.1021/jo00073a057

Reference yield:

: 91-10-1
1,3-dimethoxy-2-hydroxy-benzene

: 150563-52-3
2,6-Dimethoxy-3-nitro-4-thiocyanophenyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / Br₂, NaBr / methanol / 1 h / 0 - 5 °C

2: 99 percent / CH₃COONa / 15 h / Ambient temperature

3: 32 percent / 90percent fuming HNO₃ / acetic anhydride / 0 deg C to room temp. then room temp., 1 h

With bromine; nitric acid; sodium acetate; sodium bromide; In methanol; acetic anhydride;
DOI:10.1021/jo00073a057

Reference yield:

: 150563-50-1
2,6-dimethoxy-4-thiocyanatophenol

: 150563-52-3
2,6-Dimethoxy-3-nitro-4-thiocyanophenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / CH₃COONa / 15 h / Ambient temperature

2: 32 percent / 90percent fuming HNO₃ / acetic anhydride / 0 deg C to room temp. then room temp., 1 h

With nitric acid; sodium acetate; In acetic anhydride;
DOI:10.1021/jo00073a057