Technology Process of 11-benzyl-3-ethyl-2,4,10-trimethylprodigiosene hydrochloride
There total 6 articles about 11-benzyl-3-ethyl-2,4,10-trimethylprodigiosene hydrochloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
diethyl ether; ethanol;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 92 percent / tetrabutylammonium bromide, aqueous sodium hydroxide / CH2Cl2 / 6 h / Heating
2: 86 percent / hydrazine hydrate, potassium hydroxide / bis-(2-hydroxy-ethyl) ether / 2 h / Heating
3: 21 percent / phosphorus oxychloride / diethyl ether / 2 h / Ambient temperature
4: 79 percent / 30percent w/v palladium-on-charcoal / xylene / 2 h / Heating
5: 24 percent / HCl / ethanol; diethyl ether / 0.5 h
With
hydrogenchloride; potassium hydroxide; sodium hydroxide; tetrabutylammomium bromide; hydrazine hydrate; trichlorophosphate;
palladium on activated charcoal;
In
diethyl ether; ethanol; dichloromethane; xylene; diethylene glycol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 86 percent / hydrazine hydrate, potassium hydroxide / bis-(2-hydroxy-ethyl) ether / 2 h / Heating
2: 21 percent / phosphorus oxychloride / diethyl ether / 2 h / Ambient temperature
3: 79 percent / 30percent w/v palladium-on-charcoal / xylene / 2 h / Heating
4: 24 percent / HCl / ethanol; diethyl ether / 0.5 h
With
hydrogenchloride; potassium hydroxide; hydrazine hydrate; trichlorophosphate;
palladium on activated charcoal;
In
diethyl ether; ethanol; xylene; diethylene glycol;
