3-{(1Z,4Z,9Z,15Z)-7,12-Bis-(1-methoxy-ethyl)-3,8,13,17-tetramethyl-18-[2-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethoxycarbonyl)-ethyl]-porphyrin-2-yl}-propionic acid 2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethyl ester

Base Information

Chemical Name:3-{(1Z,4Z,9Z,15Z)-7,12-Bis-(1-methoxy-ethyl)-3,8,13,17-tetramethyl-18-[2-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethoxycarbonyl)-ethyl]-porphyrin-2-yl}-propionic acid 2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethyl ester
CAS No.:142230-12-4
Molecular Formula:C₅₆H₆₂N₄O₁₀
Molecular Weight:951.129
Hs Code.:

3-{(1Z,4Z,9Z,15Z)-7,12-Bis-(1-methoxy-ethyl)-3,8,13,17-tetramethyl-18-[2-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethoxycarbonyl)-ethyl]-porphyrin-2-yl}-propionic acid 2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethyl ester

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Chemical Property of 3-{(1Z,4Z,9Z,15Z)-7,12-Bis-(1-methoxy-ethyl)-3,8,13,17-tetramethyl-18-[2-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethoxycarbonyl)-ethyl]-porphyrin-2-yl}-propionic acid 2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethyl ester

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Technology Process of 3-{(1Z,4Z,9Z,15Z)-7,12-Bis-(1-methoxy-ethyl)-3,8,13,17-tetramethyl-18-[2-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethoxycarbonyl)-ethyl]-porphyrin-2-yl}-propionic acid 2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethyl ester

There total 3 articles about 3-{(1Z,4Z,9Z,15Z)-7,12-Bis-(1-methoxy-ethyl)-3,8,13,17-tetramethyl-18-[2-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethoxycarbonyl)-ethyl]-porphyrin-2-yl}-propionic acid 2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 553-12-8
protoporphyrin IX

: 142230-12-4
3-{(1Z,4Z,9Z,15Z)-7,12-Bis-(1-methoxy-ethyl)-3,8,13,17-tetramethyl-18-[2-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethoxycarbonyl)-ethyl]-porphyrin-2-yl}-propionic acid 2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: aq. HBr (d 1.45) / acetic acid / 72 h

2: 12 h / 20 °C

3: 94 percent / aq. NaOH / dioxane / 1 h / 70 °C

4: 33.8 percent / di-tert-butyl pyrocarbonate, pyridine, 4-dimethylaminopyridine / CHCl₃ / 0.5 h / 20 °C

With pyridine; dmap; sodium hydroxide; di-tert-butyl dicarbonate; hydrogen bromide; In 1,4-dioxane; chloroform; acetic acid;
DOI:10.1007/BF00486797

Reference yield:

: 82098-37-1
2,4-di(1-bromoethyl)deuteroporphyrin IX

: 142230-12-4
3-{(1Z,4Z,9Z,15Z)-7,12-Bis-(1-methoxy-ethyl)-3,8,13,17-tetramethyl-18-[2-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethoxycarbonyl)-ethyl]-porphyrin-2-yl}-propionic acid 2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 12 h / 20 °C

2: 94 percent / aq. NaOH / dioxane / 1 h / 70 °C

3: 33.8 percent / di-tert-butyl pyrocarbonate, pyridine, 4-dimethylaminopyridine / CHCl₃ / 0.5 h / 20 °C

With pyridine; dmap; sodium hydroxide; di-tert-butyl dicarbonate; In 1,4-dioxane; chloroform;
DOI:10.1007/BF00486797

Reference yield:

: 51589-12-9,143028-39-1,143028-40-4
protoporphyrin

: 142230-12-4
3-{(1Z,4Z,9Z,15Z)-7,12-Bis-(1-methoxy-ethyl)-3,8,13,17-tetramethyl-18-[2-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethoxycarbonyl)-ethyl]-porphyrin-2-yl}-propionic acid 2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. NaOH / dioxane / 1 h / 70 °C

2: 33.8 percent / di-tert-butyl pyrocarbonate, pyridine, 4-dimethylaminopyridine / CHCl₃ / 0.5 h / 20 °C

With pyridine; dmap; sodium hydroxide; di-tert-butyl dicarbonate; In 1,4-dioxane; chloroform;
DOI:10.1007/BF00486797