C₂₄H₂₂ClNO₃S

Base Information

Chemical Name:C₂₄H₂₂ClNO₃S
CAS No.:1315319-76-6
Molecular Formula:C₂₄H₂₂ClNO₃S
Molecular Weight:439.963
Hs Code.:

C<sub>24</sub>H<sub>22</sub>ClNO<sub>3</sub>S

Synonyms:

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Chemical Property of C₂₄H₂₂ClNO₃S

Chemical Property:

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Technology Process of C₂₄H₂₂ClNO₃S

There total 8 articles about C₂₄H₂₂ClNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₈ClNS

: 1315319-76-6
C₂₄H₂₂ClNO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 2: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.05.064

Reference yield:

: C₁₄H₁₂ClNSSi

: 1315319-76-6
C₂₄H₂₂ClNO₃S

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran

2: lithium aluminium tetrahydride / tetrahydrofuran / -40 °C

3: dichloromethane

4: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide

With copper(l) iodide; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 4: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.05.064

Reference yield:

: 959246-31-2
C₉H₅BrClNOS

: 1315319-76-6
C₂₄H₂₂ClNO₃S

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine; trifluoroacetic anhydride / dichloromethane

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 80 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran

4: lithium aluminium tetrahydride / tetrahydrofuran / -40 °C

5: dichloromethane

6: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide

With copper(l) iodide; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2: Sonogashira coupling / 6: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.05.064