nido-CyMe₂N-7-CB₁₀H₁₂

Base Information

• Chemical Name: nido-CyMe₂N-7-CB₁₀H₁₂
• CAS No.: 474377-89-4
• Molecular Formula: C₉H₂₉B₁₀N
• Molecular Weight: 259.446
• Mol file: 474377-89-4.mol

Synonyms:

Chemical Property of nido-CyMe₂N-7-CB₁₀H₁₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of nido-CyMe₂N-7-CB₁₀H₁₂

There total 1 articles about nido-CyMe₂N-7-CB₁₀H₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

nido-decaborane (17702-41-9) + Cyclohexyl isocyanide (931-53-3) + dimethyl sulfate (77-78-1) → nido-CyMe2N-7-CB10H12 (474377-89-4)

Guidance literature:

With Na₂CO₃; In benzene; cooled soln. B10H14 in benzene was treated dropwise with CyNC and left to stir for 1-2 h and brought to reflux, volatiles were removed under reduced pressure, residue was dissolved in THF and treated with Na2CO3 and (MeO)2SO2 and refluxed for 7-8 d; soln. was filtered warm, residue was warmed with warm MeCN, filtrate wasevapd., residue was washed with cold (0°C) Et2O;

DOI:10.1039/b200930g

upstream raw materials:

nido-decaborane

Cyclohexyl isocyanide

dimethyl sulfate