3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

Base Information

Chemical Name:3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al
CAS No.:99706-75-9
Molecular Formula:C₁₉H₂₀O₄S
Molecular Weight:344.431
Hs Code.:

3-<methoxy(phenylthio)methyl>-2-(3,4-dimethoxyphenyl)prop-2-en-1-al

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Chemical Property of 3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

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Technology Process of 3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

There total 4 articles about 3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 85907-71-7
3-(dimethylamino)-2-(3,4-dimethoxyphenyl)prop-2-en-1-al

: 57788-49-5
methoxy(phenylthio)methane lithium

: 99706-75-9
3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

Guidance literature:: In tetrahydrofuran; at -78 ℃; for 24h;
DOI:10.1039/c39860000075

Reference yield:

: 108-98-5
thiophenol

: 99706-75-9
3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / BF₃*OEt₂ / 1.66 h / 0 °C

2: 1.) TMEDA, sec-BuLi / 1.) THF, cyclohexane, -78 deg C, 2.5 h, 2.) THF, cyclohexane, -78 deg C, 27 h

With N,N,N,N,-tetramethylethylenediamine; boron trifluoride diethyl etherate; sec.-butyllithium;
DOI:10.1021/jo00356a025

Reference yield:

: 13865-50-4
methoxymethyl phenyl sulfide

: 85907-71-7
3-(dimethylamino)-2-(3,4-dimethoxyphenyl)prop-2-en-1-al

: 99706-75-9
3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; Yield given. Multistep reaction; 1.) THF, cyclohexane, -78 deg C, 2.5 h, 2.) THF, cyclohexane, -78 deg C, 27 h;
DOI:10.1021/jo00356a025