(3-BROMOISOXAZOL-5-YL)METHYLAMINE HYDROCHLORIDE

Base Information

• Chemical Name: (3-BROMOISOXAZOL-5-YL)METHYLAMINE HYDROCHLORIDE
• CAS No.: 90802-21-4
• Molecular Formula: C₄H₅BrN₂O*ClH
• Molecular Weight: 213.461
• Hs Code.: 2934999090
• Mol file: 90802-21-4.mol

Synonyms:5-Isoxazolemethanamine,3-bromo-, monohydrochloride (9CI); Isoxazole, 5-(aminomethyl)-3-bromo-, hydrochloride(7CI); 3-Bromo-5-(aminomethyl)isoxazole hydrochloride

Chemical Property of (3-BROMOISOXAZOL-5-YL)METHYLAMINE HYDROCHLORIDE

Chemical Property:

• Vapor Pressure: 0.000454mmHg at 25°C
• Boiling Point: 310.1oC at 760 mmHg
• Flash Point: 141.3oC
• PSA: 52.05000
• LogP: 2.39810
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

(3-Bromoisoxazol-5-yl)methylamine hydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-BROMOISOXAZOL-5-YL)METHYLAMINE HYDROCHLORIDE

There total 3 articles about (3-BROMOISOXAZOL-5-YL)METHYLAMINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N-(3-Bromo-isoxazol-5-ylmethyl)-2,2-dichloro-acetamide (105175-04-0) → 5-aminomethyl-3-bromoisoxazole hydrochloride (90802-21-4)

Guidance literature:

With hydrogen bromide; at 120 ℃; for 4h;

DOI:10.1016/S0040-4039(00)84748-6

Reference yield: 73.0%

N-dibromomethylidenehydroxylamine (74213-24-4) + N-(propargyl)-dichloroacetamide (88067-01-0) → 5-aminomethyl-3-bromoisoxazole hydrochloride (90802-21-4)

Guidance literature:

With ethereal hydrochloric acid; hydrogen bromide; potassium hydrogencarbonate; In water; N,N-dimethyl-formamide;

Reference yield:

2-methyl-propane-2-sulfinic acid (3-bromo-isoxazol-5-ylmethyl)-amide → 5-aminomethyl-3-bromoisoxazole hydrochloride (90802-21-4)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; methanol;

upstream raw materials:

N-(3-Bromo-isoxazol-5-ylmethyl)-2,2-dichloro-acetamide

N-dibromomethylidenehydroxylamine

N-(propargyl)-dichloroacetamide

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