C₃₅H₄₇BrO

Base Information

Chemical Name:C₃₅H₄₇BrO
CAS No.:172477-11-1
Molecular Formula:C₃₅H₄₇BrO
Molecular Weight:563.662
Hs Code.:

Synonyms:

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Chemical Property of C₃₅H₄₇BrO

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Technology Process of C₃₅H₄₇BrO

There total 5 articles about C₃₅H₄₇BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2,2-Dimethyl-4-((E)-tetradec-1-enyl)-[1,3]dioxolane

: 172477-11-1
C₃₅H₄₇BrO

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / H₂ / 10percent Pd/C / methanol / 760 Torr / Ambient temperature

2: 91 percent / 2 N aq. HCl / tetrahydrofuran / 2 h / Ambient temperature

3: 87 percent / pyridine, DMAP / 3 h / Heating

4: 1.) 2,6-lutidine, Tf₂O, 2.) LiBr / 1.) CH₂Cl₂, -78 deg C, 20 min, 2.) CH₂Cl₂, CH₃CN, 0 deg C, 3 h

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; dmap; trifluoromethylsulfonic anhydride; hydrogen; lithium bromide; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/0957-4166(95)00305-9

Reference yield:

: 172477-10-0
(S)-(+)-2,2-dimethyl-4-tetradecyl-1,3-dioxolane

: 172477-11-1
C₃₅H₄₇BrO

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 2 N aq. HCl / tetrahydrofuran / 2 h / Ambient temperature

2: 87 percent / pyridine, DMAP / 3 h / Heating

3: 1.) 2,6-lutidine, Tf₂O, 2.) LiBr / 1.) CH₂Cl₂, -78 deg C, 20 min, 2.) CH₂Cl₂, CH₃CN, 0 deg C, 3 h

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; dmap; trifluoromethylsulfonic anhydride; lithium bromide; In tetrahydrofuran;
DOI:10.1016/0957-4166(95)00305-9

Reference yield:

: 172587-40-5
(S)-(+)-1-triphenylmethoxyhexadecan-2-ol

: 172477-11-1
C₃₅H₄₇BrO

Guidance literature:: With 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride; lithium bromide; Yield given. Multistep reaction; 1.) CH₂Cl₂, -78 deg C, 20 min, 2.) CH₂Cl₂, CH₃CN, 0 deg C, 3 h;
DOI:10.1016/0957-4166(95)00305-9