<(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinylacetate de benzyle

Base Information

Chemical Name:<(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinylacetate de benzyle
CAS No.:95151-94-3
Molecular Formula:C₂₀H₂₅O₅P
Molecular Weight:376.389
Hs Code.:

Synonyms:

Suppliers and Price of <(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinylacetate de benzyle

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of <(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinylacetate de benzyle

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of <(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinylacetate de benzyle

There total 5 articles about <(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinylacetate de benzyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 75524-34-4
<(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinite de trimethylsilyle

: 5437-45-6
Benzyl bromoacetate

: 95151-94-3,95151-95-4
<(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinylacetate de benzyle

Guidance literature:: In benzene; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96892-9

Reference yield:

: 7306-46-9
4-chloromethyl-1,2-dimethoxy-benzene

: 95151-94-3,95151-95-4
<(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinylacetate de benzyle

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / benzene / Heating

2: 95 percent / n-BuLi / tetrahydrofuran / -60 °C

3: 90 percent / (Et₂AlH₂)Na / toluene; tetrahydrofuran

4: 75 percent / Et₃N / benzene

5: 92 percent / benzene / 1 h / Ambient temperature

With n-butyllithium; triethylamine; sodium aluminum diethyl dihydride; In tetrahydrofuran; toluene; benzene;
DOI:10.1016/S0040-4020(01)96892-9

Reference yield:

: 75524-37-7
oxyde de <(dimethoxy-3,4 phenyl)-1 ethyl>methylphospine

: 95151-94-3,95151-95-4
<(dimethoxy-3,4 phenyl)-1 ethyl> methylphosphinylacetate de benzyle

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / benzene

2: 92 percent / benzene / 1 h / Ambient temperature

With triethylamine; In benzene;
DOI:10.1016/S0040-4020(01)96892-9