1-ferrocenylisochromane

Base Information

Chemical Name:1-ferrocenylisochromane
CAS No.:620168-62-9
Molecular Formula:C₁₉H₁₈FeO
Molecular Weight:318.198
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-ferrocenylisochromane

Chemical Property:

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Technology Process of 1-ferrocenylisochromane

There total 2 articles about 1-ferrocenylisochromane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 16940-66-2
sodium tetrahydroborate

: 99994-99-7
methyl 2-(ferrocenoyl)benzeneacetate

: 7732-18-5
water

: 620168-62-9
1-ferrocenylisochromane

: 620168-63-0
2-(α-hydroxyferrocenyl)benzeneethanol

Guidance literature:: In diethyl ether; ethanol; (Ar); addn. of NaBH4 to soln. of ferrocene deriv. in 1/1 ethanol/ether, refluxing for 2 h; usual workup, elem. anal.;
DOI:10.1016/j.molstruc.2012.03.071

Reference yield: 78.0%

: 99994-99-7
methyl 2-(ferrocenoyl)benzeneacetate

: 620168-62-9
1-ferrocenylisochromane

: 620168-63-0
2-(α-hydroxyferrocenyl)benzeneethanol

Guidance literature:: With NaBH₄; In ethanol; water; NaBH4 added to Fe-comp. in a mixture of EtOH and Et2O, 1:1, v/v, refluxed for 2 h; thin-layer chromy on silica gel;
DOI:10.1107/S0108270103011703