C₃₄H₄₁ClN₆O₆S

Base Information

Chemical Name:C₃₄H₄₁ClN₆O₆S
CAS No.:1415413-56-7
Molecular Formula:C₃₄H₄₁ClN₆O₆S
Molecular Weight:697.255
Hs Code.:

C<sub>34</sub>H<sub>41</sub>ClN<sub>6</sub>O<sub>6</sub>S

Synonyms:

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Chemical Property of C₃₄H₄₁ClN₆O₆S

Chemical Property:

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Technology Process of C₃₄H₄₁ClN₆O₆S

There total 13 articles about C₃₄H₄₁ClN₆O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1263198-07-7
(3S,5R)-5-[4-(2-chlorophenyl)-2,2-dimethyl-5-oxopiperazin-1-yl]-1-(2-nitrophenyl)sulfonylpiperidine-3-carboxylic acid

: 1263264-02-3,938459-12-2
C₁₀H₁₆N₂

: 1415413-56-7
C₃₄H₄₁ClN₆O₆S

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 5h;
DOI:10.1016/j.bmcl.2012.09.103

Reference yield:

: 2,4-dioxo-3-oxa-7-azabicyclo[3.3.1]nonane-7-carboxylic acid tert-butyl ester

: 1415413-56-7
C₃₄H₄₁ClN₆O₆S

Guidance literature:: Multi-step reaction with 15 steps

1: C₂₈H₂₇F₆N₃O₃S / tetrahydrofuran / 24 h / -20 °C

2: diphenylphosphoranyl azide; triethylamine / toluene / 15 h / 90 °C

3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4: triethylamine / dichloromethane / 1 h / 20 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran / 1 h / 20 °C

6: dichloromethane / 2 h / 20 °C

7: N-chloro-succinimide / dichloromethane / 2 h / 20 °C

8: 18 h / 60 °C

9: hydrogenchloride / dichloromethane; water / 4 h / 40 °C

10: thionyl chloride / 1 h / 20 °C

11: acetic acid / toluene / 2 h / 110 °C

12: sodium cyanoborohydride / 6 h / 20 °C

13: triethylamine / dichloromethane / 5 h / 0 - 40 °C

14: sodium hydroxide; water / methanol / 0.5 h / 50 °C

15: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 20 °C

With morpholine; hydrogenchloride; N-chloro-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; C₂₈H₂₇F₆N₃O₃S; diphenylphosphoranyl azide; water; sodium cyanoborohydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2: |Curtius Rearrangement;
DOI:10.1016/j.bmcl.2012.09.103

Reference yield:

: 1415413-37-4
C₁₃H₁₇N₃O₆S

: 1415413-56-7
C₃₄H₄₁ClN₆O₆S

Guidance literature:: Multi-step reaction with 10 steps

1: dichloromethane / 2 h / 20 °C

2: N-chloro-succinimide / dichloromethane / 2 h / 20 °C

3: 18 h / 60 °C

4: hydrogenchloride / dichloromethane; water / 4 h / 40 °C

5: thionyl chloride / 1 h / 20 °C

6: acetic acid / toluene / 2 h / 110 °C

7: sodium cyanoborohydride / 6 h / 20 °C

8: triethylamine / dichloromethane / 5 h / 0 - 40 °C

9: sodium hydroxide; water / methanol / 0.5 h / 50 °C

10: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 20 °C

With hydrogenchloride; N-chloro-succinimide; thionyl chloride; water; sodium cyanoborohydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2012.09.103