(S)-4-Methyl-3-((Z)-2-{(1R,7aR)-7a-methyl-1-[(E)-(R)-1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-pent-2-enyl]-2,3,3a,6,7,7a-hexahydro-1H-inden-4-yl}-vinyl)-cyclohex-3-enol

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Chemical Name:(S)-4-Methyl-3-((Z)-2-{(1R,7aR)-7a-methyl-1-[(E)-(R)-1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-pent-2-enyl]-2,3,3a,6,7,7a-hexahydro-1H-inden-4-yl}-vinyl)-cyclohex-3-enol
CAS No.:90047-22-6
Molecular Formula:C₂₉H₄₄O₃
Molecular Weight:440.667
Hs Code.:

(S)-4-Methyl-3-((Z)-2-{(1R,7aR)-7a-methyl-1-[(E)-(R)-1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-pent-2-enyl]-2,3,3a,6,7,7a-hexahydro-1H-inden-4-yl}-vinyl)-cyclohex-3-enol

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Chemical Property of (S)-4-Methyl-3-((Z)-2-{(1R,7aR)-7a-methyl-1-[(E)-(R)-1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-pent-2-enyl]-2,3,3a,6,7,7a-hexahydro-1H-inden-4-yl}-vinyl)-cyclohex-3-enol

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Technology Process of (S)-4-Methyl-3-((Z)-2-{(1R,7aR)-7a-methyl-1-[(E)-(R)-1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-pent-2-enyl]-2,3,3a,6,7,7a-hexahydro-1H-inden-4-yl}-vinyl)-cyclohex-3-enol

There total 2 articles about (S)-4-Methyl-3-((Z)-2-{(1R,7aR)-7a-methyl-1-[(E)-(R)-1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-pent-2-enyl]-2,3,3a,6,7,7a-hexahydro-1H-inden-4-yl}-vinyl)-cyclohex-3-enol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 90047-21-5,90734-10-4,90820-38-5
(3S,10R,13R,17R)-10,13-Dimethyl-17-[(E)-(R)-1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-pent-2-enyl]-2,3,4,9,10,11,12,13,14,15,16,17-dodecahydro-1H-cyclopenta[a]phenanthren-3-ol

: 90047-22-6,90734-11-5,90820-39-6
(S)-4-Methyl-3-((Z)-2-{(1R,7aR)-7a-methyl-1-[(E)-(R)-1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-pent-2-enyl]-2,3,3a,6,7,7a-hexahydro-1H-inden-4-yl}-vinyl)-cyclohex-3-enol

Guidance literature:: In diethyl ether; benzene; for 0.3h; Irradiation;
DOI:10.1021/jo00186a014

Reference yield:

: 90047-19-1,90820-36-3,90820-42-1
C₃₇H₄₉N₃O₅

: 90047-22-6,90734-11-5,90820-39-6
(S)-4-Methyl-3-((Z)-2-{(1R,7aR)-7a-methyl-1-[(E)-(R)-1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-pent-2-enyl]-2,3,3a,6,7,7a-hexahydro-1H-inden-4-yl}-vinyl)-cyclohex-3-enol

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / lithium aluminum hydride / tetrahydrofuran / 10 h / Heating

2: 44 percent / benzene; diethyl ether / 0.3 h / Irradiation

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jo00186a014