C₆₄H₁₁₂O₁₅SSi₃

Base Information

• Chemical Name: C₆₄H₁₁₂O₁₅SSi₃
• CAS No.: 145836-85-7
• Molecular Formula: C₆₄H₁₁₂O₁₅SSi₃
• Molecular Weight: 1237.91
• Mol file: 145836-85-7.mol

Synonyms:

Chemical Property of C₆₄H₁₁₂O₁₅SSi₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₆₄H₁₁₂O₁₅SSi₃

There total 4 articles about C₆₄H₁₁₂O₁₅SSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C64H110O15SSi3 → C64H112O15SSi3 (145836-85-7) + C64H112O15SSi3

Guidance literature:

With dimethylsulfide borane complex; (R)-oxazaborolidine*BH₃; In toluene; at -10 ℃; for 12h; Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1016/S0040-4039(00)73495-2

Reference yield:

C56H96O15Si3 (131102-29-9) → C64H112O15SSi3 (145836-85-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / 1.) NaBH₄; 2.) DIEA, DMAP

2: K₂CO₃, 18-crown-6 / dimethylformamide / Ambient temperature

With dmap; sodium tetrahydroborate; 18-crown-6 ether; potassium carbonate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)73495-2

Reference yield:

C57H97F3O17SSi3 (145836-78-8) → C64H112O15SSi3 (145836-85-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃, 18-crown-6 / dimethylformamide / Ambient temperature

2: (R)-oxazaborolidine*BH₃, BH₃*SMe₂ / toluene / 12 h / -10 °C

With 18-crown-6 ether; dimethylsulfide borane complex; (R)-oxazaborolidine*BH₃; potassium carbonate; In N,N-dimethyl-formamide; toluene;

DOI:10.1016/S0040-4039(00)73495-2

upstream raw materials:

C₅₇H₉₇F₃O₁₇SSi₃

C₅₆H₉₆O₁₅Si₃

Downstream raw materials:

C₄₈H₇₂O₁₄S